Device and method for preparing metal matrix composite by adopting high-pressure gas to assist infiltration

A composite material and high-pressure gas technology, which is applied in the field of metal matrix composite material preparation devices, can solve the adverse effects of violent disturbance of metal liquid on the distribution of the second phase, affecting the stability and reliability of composite material parts, and the overflow and splash of matrix metal liquid and other issues, to achieve the effect of near-net shape, strong repeatability and uniform distribution

Active Publication Date: 2013-02-27
NEW MATERIAL INST OF SHANDONG ACADEMY OF SCI
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  • Description
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AI Technical Summary

Problems solved by technology

[0007] The pressure infiltration equipment and method adopts a mechanical device to provide one-way pressure, and the metal liquid is impregnated and formed by the pressure head (punch). Due to the sealing defect of mechanical pressing, the metal liquid of the matrix is ​​very likely to occur during the pressure infiltration forming process. Spilling and splashing will cause defects such as pores and looseness in the material, which will affect the quality of the composite material. The violent disturbance of the metal liquid will also have an adverse effect on the distribution of the second phase in the metal matrix. The unevenness of unidirectional pressure will cause local stress concentration in the composite material, which seriously affects the stability and reliability of the prepared composite parts in actual use.

Method used

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  • Device and method for preparing metal matrix composite by adopting high-pressure gas to assist infiltration
  • Device and method for preparing metal matrix composite by adopting high-pressure gas to assist infiltration

Examples

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Effect test

Embodiment 1

[0044] Example 1: Preparation of Al / Diamond composite material, the second phase Diamond particle size is 150 μm, the matrix metal is pure Al, preparation conditions: high-purity Ar in pressurized gas, temperature 800 O C, air pressure 0.55 MPa, heat preservation and pressure holding for 30 minutes.

[0045] When this embodiment is applied, refer to figure 2 , the second phase Diamond particles 20 are filled in the mold 21, the filled mold is assembled with the jacket 24 and the graphite sleeve 22, the base metal aluminum 19 is placed on the upper part of the mold, and the mold equipment is completed, the whole set of mold Installed in the heating area of ​​the induction coil 25; cover the furnace cover 13, place the temperature sensor 26 in the temperature measuring hole of the mold, and install the fastening device 14; connect the vacuum system with the vacuum valve port 28, and the pressurization and inflation system with the inflation / exhaust The valve port 12 is connect...

Embodiment 2

[0046] Example 2: Preparation of Cu / Diamond composite material, the second phase Diamond particle size is 25 μm, the matrix metal is pure Cu, preparation conditions: pressure gas 94 vol.% Ar+6 vol.% H 2 , temperature 800 O C, air pressure 3.0 MPa, heat preservation and pressure holding for 30 minutes.

[0047] The preparation process of this embodiment and embodiment 1 is basically the same, the difference is that the pressure gas adopts Ar and H 2 The mixed gas, the mixed gas composition ratio is 94 vol.% Ar+6 vol.% H 2 , so the mixing process is to open the Ar cylinder and H 2 For gas cylinders, the flow rates of the two gas paths are set to 4.70 SCM and 0.30 SCM respectively; the induction heating temperature is set to 1250 O C, the holding time is 20 min; the actual preparation pressure is 3.00 MPa, and the holding time is 10 min; under these process conditions, high-quality Cu / Diamond composite parts can be successfully prepared.

Embodiment 3

[0048] Embodiment 3: preparation Mg / SiC p Composite material, second phase SiC particle size 59 μm, matrix metal pure Mg, preparation conditions: pressure gas 99 vol.% N 2 +1 vol.% SF 6 , temperature 750 O C, air pressure 5.00 MPa, heat preservation and pressure holding for 10 minutes.

[0049] The preparation process of this example is basically the same as that of Example 1, except that the second phase filling method is SiC prepared by powder injection molding method. p Prefabricated parts; pressure gas adopts N 2 and SF 6 The mixed gas, the mixed gas composition ratio is 99 vol.% N 2 +1 vol.% SF 6 , so the aeration process is open N 2Cylinders and SF 6 For gas cylinders, the flow rates of the two gas paths are set to 4.95 SCM and 0.05 SCM respectively; the induction heating temperature is set to 750 O C, the holding time is 20 min; the actual preparation pressure is 5.00 MPa, and the holding time is 10 min; high-quality Mg / SiC can be successfully prepared under th...

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Abstract

The invention relates to a device and a method for preparing a metal matrix composite by adopting high-pressure gas to assist infiltration, and the device is formed by mutually connecting four major function systems, namely a vacuum system, a gas distribution system, a pressurizing and gas charging system and a preparation system; and the preparation method adopting the device is as follows: applying the high-pressure gas to provide pressure, driving melting matrix molten metal to effectively fill pores of a second phase or a perform and cooling so as to finally get the composite. By adopting the device and the method, structural defects can be significantly eliminated, effective control of the structure of an interface between two phases is realized through heat-keeping and pressure-keeping treatment, the performances of the composite are improved, taking the Al / diamond composite as an example, the thermal conductivity can achieve 649W / mK; through reasonable design of components of the high-pressure gas, the problems in preparation of the special metal matrix composite can be solved, and the preparation quality of the composite, including activity of matrix metal Mg, high-temperature graphitization problem of a diamond and the like, is improved; near-net-shape forming of parts in complex shapes, which are made of a large number of types of the metal matrix composites can be realized; and the preparation quality is high, and the repeatability is strong.

Description

technical field [0001] The invention relates to a metal-matrix composite material preparation device and the technical field, and provides a device and a method for preparing a metal-matrix composite material by high-pressure gas-assisted infiltration. Background technique [0002] Metal matrix composites have excellent comprehensive properties and can meet the higher comprehensive requirements for material performance in aerospace, advanced weapon systems, automobiles and electronics industries. development of. [0003] The main factors affecting the promotion and application of metal matrix composites are material properties and preparation costs. The preparation equipment and methods of composite materials determine these two aspects to a large extent. Therefore, research and development of new and efficient metal matrix composites manufacturing equipment and methods are important issues in the field of composite materials. [0004] The main preparation techniques of me...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22D19/14B22F3/26
Inventor 王西涛张洋吴建华张海龙杨滨王艳丽李甲甲
Owner NEW MATERIAL INST OF SHANDONG ACADEMY OF SCI
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