Method for producing ultrahigh-viscosity refined cotton

A technology for refining cotton and viscosity, which is applied in the fields of pulping with inorganic alkali, pulping of cellulose raw materials, textiles and papermaking, etc. The effect of low consumption and low water consumption

Inactive Publication Date: 2011-11-23
SICHUAN NITROCELLULOSE CORP
View PDF5 Cites 21 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its shortcomings are: the maturity of the selected cotton linters is high, requiring more than 80%, and it is difficult for ordinary cotton linters to reach such a high maturity; the cooking is completed by two-stage cooking, and the process is not easy to control; when bleaching, the unit Product consumed H 2 o 2 The amount is too large and within the bleaching

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for producing ultrahigh-viscosity refined cotton
  • Method for producing ultrahigh-viscosity refined cotton

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Take 300 g of cotton linters with a degree of polymerization of 2564 dp and no obvious impurities, and infiltrate it with a cooking solution. The content of NaOH in the cooking solution is 30 g / l, and the content of sodium alkylbenzene sulfonate is 0.05%. The soaked cotton linters are added to the cooking pot, and the cooking liquid is added according to the cooking liquid ratio of 1:8, the cooking pot is turned, and at the same time, the cooking liquid is heated to about 140°C with steam, and the heating time is 30 minutes. After reaching the temperature, maintain the cooking temperature at about 140°C, the cooking pressure at 0.25 MPa, and the cooking time for 2 hours; wash the absorbent cotton after cooking with tap water to remove the alkali; add tap water to the washed absorbent cotton to make the cotton-liquid ratio 3:100, Then add NaOH solution to the cotton slurry to make the pH of the cotton slurry = 9.5, then add sodium chlorite to make the concentration of sod...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a method for producing ultrahigh-viscosity refined cotton, and belongs to the technical field of refined cotton manufacture. The invention aims to provide the ultrahigh-viscosity refined cotton, the finished whiteness of which is more than 75 percent, the viscosity of which is more than 1,500mPa.s and the impurity content of which is low. The method comprises the following processes of: (1) selecting materials, opening cotton and digesting, wherein the NaOH content of the digesting solution is 20 to 45g/l, and sodium alkyl benzene sulfonate serving as an emulsifying agent is 0.05 to 0.5 weight percent; (2) pre-bleaching, wherein the concentration of sodium chlorite is 0.05 to 1 weight percent; (3) acidifying for 30 to 60 minutes when the pH is 2 to 4; (4) bleaching with hydrogen peroxide, namely washing the acidified cotton pulp, regulating the pH to be between 8 and 11, adding H2O2, and bleaching for 1 to 2 hours; and (5) drying to obtain a finished product. The ultrahigh-viscosity refined cotton product with viscosity of more than 1,500mPa.s and whiteness of more than 75 percent is produced by the method; and the method can meet the requirements of cellulose ether and cellulose ester manufacturers for producing ultrahigh-viscosity products.

Description

technical field [0001] The invention relates to a production process of ultra-high-viscosity refined cotton, more specifically relates to a production process of ultra-high-viscosity refined cotton with a viscosity greater than 1500mPa·s, and belongs to the technical field of refined cotton production. Background technique [0002] When cellulose ether and cellulose ester manufacturers produce high-viscosity products, they always require that the raw material—refined cotton—reach a certain degree of whiteness, and the higher the viscosity, the better, so as to meet their requirements for producing high-viscosity products. Traditional refined cotton production generally adopts the following processes: 1) Cotton linters are opened; 2) High-pressure cooking: add cotton linters to the cooking pot, add lye to heat up and cook; 3) Washing: Cook the cotton linters washing; 4) pretreatment before bleaching; 5) bleaching; 6) rolling and drying to obtain the finished product. Such as...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): D21C3/02D21C3/22D21C9/14D21C9/16
Inventor 张仁旭阳洪赵利斌郭朝刚马君吴定军郭逢文
Owner SICHUAN NITROCELLULOSE CORP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products