Biological degradable self-expansive fallopian tube intrauterine device produced by natural synthesis composite materials
A technology for composite materials and IUDs, which is applied in the field of preparing biodegradable self-expandable fallopian tube IUDs from natural and synthetic composite materials, achieving the effects of short preparation process, high economic benefits and simple operation
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Embodiment 1
[0035] A method for preparing a biodegradable self-expandable fallopian tube IUD from natural and synthetic composite materials, comprising the steps of:
[0036] (1) 100,000 polylactic acid with a molecular weight of 99Kg and 1Kg of aluminum-free baking powder are dissolved in chloroform, and a uniform solution is obtained under stirring. The mass ratio of polylactic acid with a molecular weight of 100,000 and chloroform is 5:95;
[0037] (2) Place the solution obtained in step (1) in an oven, and foam at 75°C for 60 minutes to obtain a degradable self-expanding sponge-like structure;
[0038] (3) Cut the spongy structure into a cylinder with a diameter of 1.0 mm and a length of 40 mm, then soak it in an aqueous chitosan solution with a mass concentration of 3%, soak for 30 minutes, and take it out to obtain a natural and synthetic compound Materials to prepare biodegradable self-expandable fallopian tube IUD.
[0039] The IUD is compressible with a diameter compression rat...
Embodiment 2
[0041] A method for preparing a biodegradable self-expandable fallopian tube IUD from natural and synthetic composite materials, comprising the steps of:
[0042] (1) Polylactic acid with 130,000 molecular weight of 99Kg and 1Kg food-grade sweet baking powder are dissolved in chloroform, obtain uniform solution under stirring, the mass ratio of polylactic acid with molecular weight 130,000 and chloroform is 10: 90;
[0043] (2) Place the solution obtained in step (1) in an oven, and foam at 25°C for 120 minutes to obtain a degradable self-expanding sponge-like structure;
[0044] (3) Cut the spongy structure into a cylinder with a diameter of 0.3 mm and a length of 10 mm, then soak it in an aqueous chitosan solution with a mass concentration of 5%, soak for 30 minutes, and take it out to obtain a natural and synthetic compound Materials to prepare biodegradable self-expandable fallopian tube IUD.
[0045] The IUD is compressible, and the compression ratio of the diameter is ...
Embodiment 3
[0047] A method for preparing a biodegradable self-expandable fallopian tube IUD from natural and synthetic composite materials, comprising the steps of:
[0048] (1) Polylactic acid with a molecular weight of 150,000 of 98Kg and 2Kg food grade aluminum-free baking powder are dissolved in chloroform, and a uniform solution is obtained under stirring. The mass ratio of polylactic acid with a molecular weight of 150,000 and chloroform is 15 : 85;
[0049] (2) Place the solution obtained in step (1) in an oven and foam at 120°C for 5 minutes to obtain a degradable self-expanding sponge-like structure;
[0050] (3) Cut the spongy structure into a cylinder with a diameter of 0.5 mm and a length of 30 mm, then soak it in an aqueous chitosan solution with a mass concentration of 7%, soak for 30 minutes, and take it out to obtain a natural and synthetic compound Materials to prepare biodegradable self-expandable fallopian tube IUD.
[0051] The IUD is compressible with a diameter co...
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