Apparatus and method for determining high temperature wettability

A technology of wettability and high temperature, which is applied in the direction of measuring devices, furnaces, instruments, etc., can solve the problem that it is difficult to measure the initial contact angle of the system and the kinetics of droplet spreading at isothermal conditions, and the metal samples are easy to oxidize and cannot truly reflect the melting of metals. Eliminate stress, improve test accuracy, and reduce pollution

Inactive Publication Date: 2012-02-15
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

In this new technology, there's an improved way to measure how well molten aluminum (Al) falls into liquid when poured onto another material like steel). By separating the hot spot caused by melting off some parts of the copper plate called iron spots, we get ridges along its edges where impurities may come out. To prevent such issues, the current methods involve removing any unwanted substances before adding them to the mixture. Additionally, the use of specific techniques helps create clear images without distortion due to uneven distribution of atoms near certain points within the atom cloud. These technical improvements make measurements more accurate than previous methods while also improving efficiency compared to older methods.

Problems solved by technology

This patented technical problem addressed in this patents relates to real time measurements of liquid crystal compound (LC) surfaces with different properties like hydrophilicity/wettabilities at various temperatures. Existing techniques have limitations due to factors like oxidization caused by oxygen from air exposure and impurity levels within the LSZ layer itself.

Method used

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  • Apparatus and method for determining high temperature wettability
  • Apparatus and method for determining high temperature wettability
  • Apparatus and method for determining high temperature wettability

Examples

Experimental program
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Effect test

Embodiment

[0062] Embodiment: at 1000 ℃ and purity is 99.999% and the wettability of measuring pure Al on SiC substrate under the Ar gas protection of purification treatment (referring to Figure 1 to Figure 4 ).

[0063] 1. Adjust the position of He-Ne laser light source 21 and CCD digital camera or CMOS high-speed camera 23, so that CCD digital camera or CMOS high-speed camera 23 lens, quartz glass observation window 13, middle shield layer middle position wall through hole, heating body 16 The through hole of the heating body and the axis of symmetry of the He-Ne laser light source 21 are on the same horizontal line. Adjust the focal length of CCD digital camera or CMOS high-speed video camera 23 lenses.

[0064] 2. Open the fastening bolts connecting the lower end of the drip tube support flange 7 and the welding flange on the upper end of the upper cover 3, remove the drip tube support flange 7, and take out the drip tube 9 made of high-purity alumina.

[0065] Open the furnace co...

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PUM

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Abstract

The invention discloses an apparatus and a method for determining high temperature wettability. The apparatus comprises a heater body, a heating portion, an extruding dripping portion, a sample supporting portion and an image acquisition and processing portion. The heater body is comprised of a stainless steel cavity, a furnace lid and a No. 3 fluorine rubber ring bolt connecting together. A shielding layer in the heating portion is arranged in the center of a furnace bottom in the heater body, and a heating member is placed at the center of the shielding layer. The extruding dripping portionis perpendicularly arranged on an upper end of the heater body, and a lower end of a thermocouple in the heating portion, a lower end of the extruding dripping portion and an upper end of a sample bench are placed in the heater body. A substrate is placed at top of the sample bench. Two sets of CCD digital cameras or CMOS high speed cameras in the image acquisition and processing portion and a light source are respectively placed at the front and rear and the left and right of the heater body, and are in a same horizontal line with a symmetric axis of a quartz glass observation window, a wallthrough hole on the shielding layer and a heating member through hole on the heating member. The invention also provides a method for determining high temperature wettability.

Description

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Claims

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Application Information

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Owner JILIN UNIV
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