Method for eliminating carbon contamination of precious metal components
A part, platinum metal technology, used in the field of connecting precious metal parts, which can solve problems such as molten glass contamination
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[0049] The test sample (sample 1 ) in the form of a bag was made from two 0.762 mm thick plates of 90% platinum-10% rhodium alloy. A 10 mg sample of carbon was sealed in the bag by welding the edge of the plate. Then, the sample was immersed in a molten glass bath (EagleXG manufactured by Corning Incorporated) at 1450°C TM glass) for 24 hours. Sample 1 ( Figure 8 ) without prior heat treatment of the platinum-rhodium alloy according to the embodiments described herein prior to immersion. Figure 8 Shows the generation of a large number of blisters (bubbles) at the surface of the sealed metal bag due to high temperature immersion.
[0050] For comparison, another sample (Sample 2) was made in the same manner as Sample 1, and also had 10 mg of carbon placed in a sealed bag. Sample 2 was immersed in molten EagleXG at the same 1450°C as per Sample 1 TM Heat treatment at 1450°C for 7 days (168) hours before the glass bath. Figure 9 Sample 2 after being immersed in molten gl...
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