Cryoconcentration method for adding dimethyl dicarbonate into fruit juice

A technology of dimethyl dicarbonate and dimethyl dicarbonate content, which is applied in the field of low-temperature concentration, can solve the problems of easy taste change, aroma loss, fruit juice spoilage, etc., and achieve the prevention of spoilage and fruit juice concentration The effect of simple method

Active Publication Date: 2012-06-27
汕尾市华亿食品科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, some heat-sensitive fruit juices are concentrated at this temperature, which is prone to problems such as taste change, color change, and serious loss of aroma. Using higher vacuum and low-...

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0032] Use the EYELA SB-1000 rotary evaporator to concentrate lychee juice. First, turn on the matching HX-1050 rotary evaporator steam condensate cooling and circulation switch, set the cooling water temperature to 10°C, and add the soluble solid content to the 500ml rotary flask For 14.9% lychee juice in 200ml, turn on the DTC-22B diaphragm vacuum pump, wait until the vacuum degree drops to 1.5kpa, turn on the rotating device of the rotary evaporator, start to concentrate, use the vacuum suction tube that comes with the rotary evaporator, and inhale 10 μl of dimethylformamide The ethanol solution 1ml of base dicarbonate is concentrated to about 140ml liquid in the receiving bottle, stops concentrating, and the lychee juice in the rotating flask is poured out, and now 45ml of lychee concentrated juice is collected, and the soluble solid content reaches 58.8%.

Embodiment 2

[0034] Wiped film thin film evaporator ( Produced by Wuxi Huasheng Pharmaceutical Engineering Equipment Co., Ltd. ) To concentrate the mulberry juice, first turn on the cooling ice water circulation system, set the temperature of the cold water to 10°C, set the temperature of the hot water to 30°C, prepare 50L of mulberry fruit juice with a soluble solid content of 9.1%, and add 2ml of distillate to the mulberry juice. Methyl dicarbonate, stir well. Turn on the Rhodes-water ring vacuum pump, and adjust the vacuum degree of the vacuum concentration equipment to 1kpa. Turn on the feed pump, and pump the prepared mulberry juice added with dimethyl dicarbonate into the rotary scraping film concentration device. Set the feeding pump speed to 20L / hr. After all the materials have been fed in, collect the concentrated mulberry juice from the substrate concentration pot to obtain 24L concentrated mulberry juice. The soluble solid content of the concentrated mulberry juice is 21.9%.

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Abstract

The invention discloses a cryoconcentration method for adding dimethyl dicarbonate into fruit juice, which comprises the following steps that: 1) the temperature of a cooling medium in a condenser in a vacuum concentrator is adjusted below 10 DEG C; 2) fruit normal juice is added into a vacuum concentration container, and is vacuumized to the absolute pressure which is lower than 2kPa; 3) a container is utilized to absorb dimethyl dicarbonate in a vacuum way; and 4) the fruit juice is heated and concentrated, the heating temperature is not higher than 30 DEG C, and the solid content of the fruit juice is concentrated to 20-60%, wherein the amount of the dimethyl dicarbonate which is absorbed in the step 3) is that: the concentration of the dimethyl dicarbonate in the fruit juice before the fruit juice is concentrated is 10-50ppm. The fruit juice concentration method is simple and practicable, and can simultaneously prevent the fruit juice from spoilage during the concentration process.

Description

technical field [0001] The invention relates to a low-temperature concentration method for adding dimethyl dicarbonate to fruit juice. Background technique [0002] Concentrated fruit juice is a kind of product produced by fruit juice, sterilization, concentration, filling and other processes. Concentrated fruit juice is the main raw material for the development of fruit juice drinks, fruit wine, fruit vinegar and other fruit processing products. Concentrated fruit juice has the characteristics of small size, convenient transportation, and low packaging cost, especially as a fruit juice variety for international trade. [0003] At present, the most commonly used method of concentration is vacuum concentration. The boiling point of vacuum concentration is negatively correlated with the degree of vacuum. In theory, the boiling point of water at 1kpa vacuum is 6.97°C, 2kpa is 17.50°C, 3kpa is 24.08°C, 5kpa is 32.87°C, and 10kpa is 32.87°C. It is 45.81°C, because water vapor is...

Claims

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Application Information

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IPC IPC(8): A23L2/10
Inventor 徐玉娟吴继军温靖肖更生林羡陈于陇李升锋唐道邦张岩
Owner 汕尾市华亿食品科技有限公司
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