Preparation method of polyurethane foam material

A technology of polyurethane foam and foam opening, which is applied in the field of polyurethane foam material preparation, can solve the problems of emulsified particle precipitation, far away from the production site, and no more than two days, so as to alleviate particle precipitation, reduce radiation factor, and low thermal conductivity. Effect

Active Publication Date: 2012-07-11
ANHUI KONKA TONGCHUANG HOUSEHOLD APPLIANCES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the polyurethane foaming system commonly used by enterprises is generally a ground tank type combined polyether and cyclopentane storage method, that is, the foaming additive is sent to the cyclopentane ground tank by the delivery pump, and the circulating pump performs repeated self-circulation. Mix the additive and cyclopentane evenly, and then send it to the static mixer through the pipeline. At the same time, the prepared combined polyether is also delivered to the static mixer. After the three are mixed evenly, they are sent to the high-pressure generator through the pipeline. In the foaming equipment, the ground tank device used in this storage method is large in volume, far away from the production site, and the transportation pipeline is long, which requires a long foaming system pipeline for transportation. In addition, cyclopentane, additives, and combined polyether are uniformly formed by stirring The storage time of the emulsion should not exceed two days. After two days, the emulsified particles of the FA-188 additive will precipitate seriously, so the performance cannot meet the needs of flexible production.

Method used

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  • Preparation method of polyurethane foam material
  • Preparation method of polyurethane foam material
  • Preparation method of polyurethane foam material

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preparation example Construction

[0034] The embodiment of the present invention discloses a preparation method of polyurethane foam, comprising:

[0035] Step a) mixing the combined polyether and cyclopentane to obtain a mixture;

[0036] Step b) mixing the mixture, foaming additive and polyisocyanate in a foaming gun, and reacting and foaming to obtain a polyurethane foam material.

[0037] The foaming additive described in the present invention preferably adopts FA-188 type foaming additive.

[0038] Such as figure 1 As shown, it is a schematic diagram of the preferred foaming gun used in the present invention figure 1 ,include:

[0039] Foaming port 106;

[0040] The black material inlet pipe 103 that links to each other with foaming mouth 106, is used for polyisocyanate feeding;

[0041] The injection valve 107 connected to the foaming port 106 through the static premixer 108;

[0042] The foaming additive inlet pipe 105 and the white material inlet pipe 101 that are connected with the injection val...

Embodiment 1

[0064] Step a) mixing 100 grams of combined polyether produced by Nanjing Hongbaoli Co., Ltd. and 13.5 grams of cyclopentane produced by Meilong Cyclopentane Chemical Co., Ltd. to obtain a mixture;

[0065] Step b) the FA-188 type foaming additive of described mixture, 3.8 gram 3M companies is mixed in the injection valve of foaming gun, then add and add 140 gram polyisocyanates by the black material inlet pipe of foaming gun, reaction foaming After 3 minutes, a polyurethane foam material was obtained.

[0066] Utilize moisture tester, viscosity tester, universal testing machine, thermal conductivity meter etc. to test the polyurethane foam material prepared in this embodiment respectively, the packing density of described polyurethane foam material is 38.9kg / m 3 , heart density is 33.2kg / m 3 , the parallel compressive strength is 0.20Mpa, the vertical compressive strength is 0.16Mpa, and the thermal conductivity is 20.6mW / m·K. Such as image 3 Shown is the SEM photo of the...

Embodiment 2

[0068] Step a) mixing 100 grams of model BJ2-3879 combined polyether with 13.5 grams of cyclopentane to obtain a mixture;

[0069] Step b) mix described mixture and 3.85 grams of FA-188 type foaming additives in the static premixer of foaming gun, then add 140 grams of polyisocyanates through the black material inlet pipe of foaming gun, react and foam for 4 minutes , to obtain polyurethane foam.

[0070] Utilize moisture tester, viscosity tester, universal testing machine, thermal conductivity meter to test the polyurethane foam material prepared in this embodiment, the packing density of described polyurethane foam material is 38.9kg / m 3 , the heart density is 33.0kg / m 3 , the parallel compressive strength is 0.20Mpa, the vertical compressive strength is 0.16Mpa, and the thermal conductivity is 19.5mW / m·K.

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Abstract

The embodiment of the invention discloses a preparation method of a polyurethane foam material and a foaming gun. The preparation method comprises: mixing combined polyether and cyclopentane to prepare mixture; and mixing the mixture, foaming additives and polyisocyanate in the foaming gun for reaction to generate foam, thereby obtaining the polyurethane foam material. The polyurethane foam material is prepared according to the principle of the high-pressure foaming gun and can be freely prepared for use in areas near the production place due to the flexibility in operation of the high-pressure foaming gun, particle precipitation can be reduced, and no long-distance transportation pipeline is needed for transportation. Moreover, the foaming additives can become ultra-fine crystal nucleus during foraming of polyurethane to promote chemical reaction of the polyisocyanate and combined polyether to form a fine porous structure, the radiation factor of the polyurethane foam material is reduced, and the prepared polyurethane foam material has a lower thermal conductivity coefficient.

Description

technical field [0001] The invention relates to the technical field of foam materials, in particular to a preparation method of polyurethane foam materials. Background technique [0002] Environmental protection, energy saving and sustainable development are the themes of the development of all countries in the world today. In the field of refrigerators in the home appliance industry, with the continuous progress of energy-saving technology, the improvement of the energy consumption level of refrigerator products will be a bottleneck affecting the development of the refrigerator field. [0003] The heat transfer of the polyurethane foam material used on the refrigerator box mainly comes from three aspects: gas heat transfer, polyurethane matrix heat transfer and foam radiation heat transfer, of which gas heat transfer accounts for 50%, polyurethane matrix heat transfer accounts for 20%, Foam radiative heat transfer accounts for 30%. The heat transferred by foam radiation c...

Claims

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Application Information

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IPC IPC(8): C08J9/14C08G18/48B05B7/04
Inventor 陈家谦
Owner ANHUI KONKA TONGCHUANG HOUSEHOLD APPLIANCES
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