Preparation process for prinsepia utilis royle grease

A preparation process, a technology of green thorn fruit, which is applied in the directions of oil/fat production and fat production, can solve problems such as storage difficulties, easy oxidation of oil products, natural quality damage, etc. The effect of low extraction temperature

Inactive Publication Date: 2012-08-08
华健 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The oil yield rate of cold pressing technology is low, and the crude oil needs to be refined through decolorization, deacidification, deodorization, etc. The whole process is in an aerobic environment, and the fatty acid structure in the green thorn fruit oil changes through the

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A kind of preparation technology of green sorrel oil, is characterized in that it comprises the steps:

[0028] (1), remove the pericarp from the collected green thorn fruit, and wash it with clean water;

[0029] (2), avoid direct sunlight to dry or dry the clear water on the surface of the fruit after washing;

[0030] (3), after roasting at 90°C for 120 minutes, take a sample and measure its moisture content with a moisture analyzer, and the moisture content is 8.2%;

[0031] (4), pulverize with pulverizer then, and cross 40 mesh sieves;

[0032] (5), put the green thorn fruit raw material after crushing and sieving: the extraction pressure of carbon dioxide is 15Mpa, and the flow rate of carbon dioxide in the extraction kettle of 38°C is 50L / hr, and the extraction time is 150min for supercritical extraction;

[0033] (6), the material obtained in the fifth step is separated at a separation pressure of 5Mpa and a separation temperature of 60° C. in a separation tan...

Embodiment 2

[0035] A kind of preparation technology of green sorrel oil, is characterized in that it comprises the steps:

[0036] (1), remove the pericarp from the collected green thorn fruit, and wash it with clean water;

[0037] (2), avoid direct sunlight to dry or dry the clear water on the surface of the fruit after washing;

[0038] (3), after roasting at 100°C for 90 minutes, take a sample and measure its moisture content with a moisture analyzer, and the moisture content is 6.7%;

[0039] (4), pulverize with pulverizer then, and cross 60 mesh sieves;

[0040] (5), put the green thorn fruit raw material after crushing and sieving: the extraction pressure of carbon dioxide is 40Mpa, and the flow rate of carbon dioxide in the extraction kettle of 45°C is 300L / hr, and the extraction time is 100min for supercritical extraction;

[0041] (6), the material obtained in the fifth step is separated at a separation pressure of 6Mpa and a separation temperature of 38°C in a separation tank...

Embodiment 3

[0043] A kind of preparation technology of green sorrel oil, is characterized in that it comprises the steps:

[0044] (1), remove the pericarp from the collected green thorn fruit, and wash it with clean water;

[0045] (2), avoid direct sunlight to dry or dry the clear water on the surface of the fruit after washing;

[0046](3), after roasting at 120°C for 30 minutes, take a sample and measure its moisture content with a moisture analyzer, and the moisture content is 9.6%;

[0047] (4), pulverize with pulverizer then, and cross 100 mesh sieves;

[0048] (5), put the green thorn fruit raw material after crushing and sieving: the extraction pressure of carbon dioxide is 25Mpa, and the flow rate of carbon dioxide in the extraction kettle with extraction temperature of 60°C is 5000L / hr, and the extraction time is 30min for supercritical extraction;

[0049] (6), the material obtained in the fifth step is separated at a separation pressure of 7Mpa and a separation temperature ...

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PUM

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Abstract

The invention provides a preparation process for prinsepia utilis royle grease. The preparation process comprises the following steps: firstly, peeling the collected prinsepia utilis royle grease fruits, elutriating the peeled prinsepia utilis royle grease fruits with clear water and cleaning; secondly, keeping the clear water on the surfaces of the fruits cleaned by elutriating away from being dried in the sun or dried in the air by sunlight direct irradiation; thirdly, parching the fruits at the temperature of 90-120DEG C for 30-180 minutes; fourthly, crushing the parched fruits by using a crushing machine and sieving the crushed fruits through a sieve with 40-100 meshes; fifthly, feeding the crushed and sieved prinsepia utilis royle raw materials into an extraction kettle and carrying out supercritical extraction; and sixthly, separating the materials obtained in the fifth step in a separation kettle with the separation pressure of 5-12Mpa and the temperature of 38-60DEG C. According to the method, prinsepia utilis royle grease can be obtained on the premise that a fatty acid structure is not damaged and has favorable permeability and easiness in absorption.

Description

technical field [0001] The invention relates to a preparation process of green thorn fruit oil. Background technique [0002] Supercritical fluid extraction technology has been researched and developed for more than 100 years. my country has introduced supercritical fluid extraction technology since the 1980s and studied it. The basic principle of this technology is to use carbon dioxide under a certain pressure and temperature, which has both good gas diffusivity and liquid solubility, to extract active ingredients from animal and plant raw materials, and realize separation and collection through pressure and temperature control. Supercritical CO 2 The extraction technology has the advantages of low extraction temperature, high extraction efficiency, no solvent residue, no pollution discharge, high product quality, etc. It is one of the more advanced extraction and separation technologies in the world at present. [0003] Prinsepia utilis royle, Latin name Prinsepia utili...

Claims

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Application Information

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IPC IPC(8): C11B1/10C11B1/04
Inventor 华健曾智平
Owner 华健
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