Method for preparing antibacterial non-woven fabrics based on nano-silver monoatomic antibacterial agent
A non-woven fabric and nano-silver technology, applied in non-woven fabrics, textiles and papermaking, rayon manufacturing, etc., can solve the problems of inability to obtain high antibacterial properties, limited antibacterial and antiviral properties, etc.
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Embodiment 1
[0085] 1. Preparation of ultrafine silver elemental inorganic antibacterial agent powder
[0086] According to the record of Example 6 in the ZL 200910091031.1 instruction manual, a silver sol containing 16-38nm silver particles and a concentration of 10000ppm was prepared, and then spray-dried using the LDZ spray drying equipment of Wuxi Dongsheng Spray Granulation Drying Machinery Factory, and then used in Shanghai The LQ fluidized bed jet mill of Saishan Powder Machinery Manufacturing Co., Ltd. is used for pulverization and classification to produce ultrafine powder of pure silver elemental inorganic antibacterial agent with a particle size of 80-100nm.
[0087] 2. Preparation of elemental silver-containing antibacterial masterbatch
[0088] Get 10kg of the gained elemental silver antibacterial agent and add it to a high-speed mixer, then add 0.2kg of discoloration inhibitor natural hydrotalcite, and process it at a high speed for 15 minutes at a speed of 3000 rpm. Then add ...
Embodiment 2
[0092] 1. Preparation of ultrafine silver elemental inorganic antibacterial agent powder
[0093] According to the record of Example 5 in the ZL 200910091031.1 specification, a silver sol containing 10-35nm silver particles and a concentration of 5000ppm was prepared, dried with a nano-scale spray dryer from Buchi, Switzerland, and then produced by Qingdao Jingjing Micro Powder Equipment Co., Ltd. The QLM-3 airflow milling and classifying machine is used for crushing and classifying, and the pure silver elemental inorganic antibacterial agent is produced, and the particle size is 80-100nm.
[0094] 2. Preparation of elemental silver-containing antibacterial masterbatch
[0095] Get 3kg of elemental silver antibacterial agent and add it to a high-speed mixer, then add 0.015kg of calcined product [MgO. . Then add 0.5kg of coupling dispersant SG-Al821 distearoyloxyisopropyl aluminate, then add 85kg of PP resin, and mix with a high-speed mixer at a low speed of 600 rpm for 3 min...
Embodiment 3
[0099] 1. Preparation of ultrafine silver elemental inorganic antibacterial agent powder
[0100] According to the record of Example 7 in the ZL 200910091031.1 instruction manual, a silver sol containing 12-30nm silver particles with a concentration of 20000ppm was prepared, and after spray drying, it was pulverized and classified to obtain a pure silver elemental inorganic antibacterial agent with a particle size of 10-80nm .
[0101] 2. Preparation of elemental silver-containing antibacterial masterbatch
[0102] Get 20kg of elemental silver antibacterial agent and add it to a high-speed mixer, then add 1kg of discoloration inhibitor benzotriazole and 1kg of aluminum silicate, and process it at a high speed of 3500 rpm for 30 minutes. Then add 1 kg of aluminum-titanium composite coupling dispersant, then add 90 kg of PP resin, and mix at a low speed of 600 rpm for 5 minutes until the materials are evenly mixed. Release the material. Add the extruder to extrude and granula...
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