Application of sunitinib in preparation of acetylcholinesterase inhibitor
A technology of acetylcholinesterase and sunitinib, which is applied in the field of anti-tumor drugs and can solve the problems such as sunitinib that have not yet existed
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[0017] Detection of sunitinib (compound 1) inhibiting acetylcholinesterase activity
[0018] The sunitinib (compound 1) used in the test of the present invention was prepared according to the method reported in the literature: WO 99 / 48868 (publication date: September 30, 1999).
[0019]
[0020] Inhibition of acetylcholinesterase activity detection test:
[0021] Fresh acetylcholinesterase, purchased from Sigma company;
[0022] Thioacetylcholine salt (ATOH) was purchased from Sigma as a substrate;
[0023] 5,5-dithiobis(2-nitrobenzoic acid) (DTNB) is a chromogen, purchased from Sigma;
[0024] 0.01M phosphate buffer (pH=7.0);
[0025] Sunitinib was made into DMSO solution (both 20 μmol / mL).
[0026] Detection method:
[0027] (1) Acetylcholinesterase and substrate are mixed with 0.01M phosphate buffer to prepare a suitable concentration solution. 1ml of the initial reaction system contains 0.02 units of enzyme, 0.1 μmol of substrate, 0.1 μmol of chromogen, and 10 μL o...
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