Heat pump type low-temperature evaporating device and method

A technology of low-temperature evaporation and heat pump, which is applied in the field of low-temperature evaporation process and equipment, heat pump energy saving, can solve the problems of low boiling point of organic solvents, pollute the environment, inflammable and explosive, etc., achieve light equipment corrosion, low evaporation temperature, and reduce gas emissions Effect

Inactive Publication Date: 2012-10-03
DALIAN UNIV OF TECH
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

Compared with water as an extractant, the extraction effect of organic solvents is superior. In recent years, the use of organic solvents in the extraction process has been increasing, but organic solvents have the characteristics of low boiling point, flammable, explosive, toxic, and pollute the environment.

Method used

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  • Heat pump type low-temperature evaporating device and method

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Embodiment 1

[0019] like picture As shown, the heat transfer area of ​​the feed-liquid evaporator is 0.58m 2 , the steam condenser area is 1.58 m 2 , The compressor uses the Copeland CRNQ-0500-TFO-272 type fully enclosed 5-hp compressor, and the throttling device uses a thermal expansion valve. Using R22 as heat medium, evaporate and concentrate 10.5% glucose solution.

[0020] Material circulation: the non-condensable gas is pumped out by the vacuum pump on the top of the condensate tank to maintain the system pressure between 2.5-5kPa, the thinner liquid is pumped into the evaporator until the liquid level of the separator reaches the specified height, and the spray volume of the pumped liquid is 300L / h The film distributor on the top of the evaporator is evenly distributed to the heat transfer tubes of the evaporator and flows down in the form of a film. The liquid film absorbs the heat of the heat medium steam outside the tube and evaporates at the evaporation temperature between 28°...

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Abstract

The invention relates to a heat pump type low-temperature evaporating device and method, belonging to the technical fields of chemical separation, energy conservation and emission reduction. The method is characterized in that a solvent is evaporated and condensed in the heating circulation process of a heat-carrying medium, so that the aim that a thermosensitive material liquid is evaporated and concentrated or an organic solvent is recovered at the low temperature can be achieved; the heat pump type low-temperature evaporating device mainly comprises a material liquid evaporator, a gas-liquid separator, a secondary steam condenser, a condensate tank, a heat medium storage tank, a heat medium steam compressor, a filter, a material liquid pump, a condensate pump, a throttling device and a pipeline valve, wherein a single-effect or multi-effect falling-film evaporator is used as the material liquid evaporator. The material liquid evaporating temperature is controlled to be within the range of 25-60 DEG C by adjusting the system vacuum degree; and the system heating capacity is controlled to be matched with the evaporation capacity by adjusting the input power of the compressor at the variable frequency. The heat pump type low-temperature evaporating device and method have the beneficial effects and advantages that the gas emission is reduced, so that the environment is protected, and the energy is saved; and furthermore, the active ingredients of the material liquid can be maintained by low-temperature evaporation, equipment is seldom corroded, and a pipeline is not easily blocked, so that the equipment cost is lowered.

Description

technical field [0001] The invention belongs to the technical field of chemical separation and energy saving and emission reduction, and relates to a low-temperature evaporation process and device for recovering heat-sensitive materials and low-boiling solvents, and in particular to a heat pump energy-saving technology coupled with heat medium heating cycle, solution evaporation, and solvent condensation. Background technique [0002] In the evaporation and concentration operation, when heat-sensitive materials encounter high temperature, their active ingredients will be denatured or scarred on the evaporation wall, which will affect the evaporation efficiency and product quality. Therefore, the influence of evaporation temperature is a very important control condition. For example, in the biomedicine and food industry, some of its products are not resistant to high temperatures, that is, heat-sensitive materials need to be evaporated under low temperature conditions. In low...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D1/26B01D1/30
Inventor 马学虎张卓敏兰忠白涛林载祁
Owner DALIAN UNIV OF TECH
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