Method for preparing biological aviation fuel by utilizing cornus wilsoniana oil
A technology for light bark oil and aviation fuel, which is applied in the field of preparing bio-aviation fuel by utilizing light bark oil, and achieves good economic and social benefits and the effects of improving quality
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Embodiment 1
[0030] This embodiment includes the following steps:
[0031] (1) Filter the eucalyptus oil to remove particulate impurities, add softened water at the same temperature after heating to 70°C (the weight of the added demineralized water is 3% of the weight of the eucalyptus oil), stir for 30 minutes, and then use 3000r Centrifuge at a speed of 1 / min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 3 hours to obtain refined eucalyptus oil;
[0032] (2) After cooling the refined eucalyptus oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to perform a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is NiO-MoO 3 / γ-Al 2 o 3 Catalyst, the amount of which is equivalent to 3% of the weight of the obtained refined eucalyptus oil, the temperature is raised to 400°C, the absolute pressure is 4MPa, and hydrogen is introduced at the same time, the hydrogen-oil vol...
Embodiment 2
[0038] This embodiment includes the following steps:
[0039] (1) Filter the eucalyptus oil to remove small particle impurities, heat to 70°C, then add demineralized water at the same temperature (the weight of demineralized water added is 3% of the oil weight), stir for 30 minutes, and then use 3000r / Centrifuge at a speed of 1 min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 3 hours to obtain refined eucalyptus oil;
[0040] (2) After cooling the refined eucalyptus oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to carry out a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is CoO-MoO 3 / γ-Al 2 o 3 Catalyst, the amount of which is equivalent to 2% of the weight of the obtained refined eucalyptus oil, the temperature is raised to 380 ° C, the absolute pressure is 5 MPa, and hydrogen is introduced at the same time, the volume ratio of hydrogen to...
Embodiment 3
[0044] This embodiment includes the following steps:
[0045] (1) Filter the eucalyptus oil to remove small particle impurities, heat to 70°C, then add demineralized water at the same temperature (the weight of demineralized water added is 3% of the oil weight), stir for 30 minutes, and then use 3000r / Centrifuge at a speed of 1 min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 3 hours to obtain refined eucalyptus oil;
[0046] (2) After cooling the refined eucalyptus oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to perform a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is NiO-WO 3 / ZSM-5 catalyst, the amount of which is equivalent to 5% of the weight of the obtained refined eucalyptus oil, the temperature is raised to 400°C, the absolute pressure is 3.5MPa, and hydrogen is introduced at the same time, the volume ratio of hydrogen to oil is 900...
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