High-strength and high-plasticity magnesium alloy material and preparation method thereof

A technology of alloy material and magnesium alloy, which is applied in the field of high-strength and high-plasticity magnesium alloy material and its preparation, can solve the problems of high rare earth content, high cost, and poor market competitiveness, and achieve wide sources, high strength and plasticity, and improved The effect of strength and plasticity

Inactive Publication Date: 2012-11-21
刘利涛 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the research results of these universities, research institutes and enterprises have common shortcomings, that is, the rare earth content in magnesium alloy is relatively high, basically reaching more than 20%, and the plasticity is poor, basically below 5%.
The high content of rare earth elements leads to high material cost and poor market competitiveness; poor plasticity limits its application field and scope
The combination of these factors has led to the fact that these materials are still in the laboratory stage, and it is difficult to produce in large quantities. At the same time, magnesium alloys with high strength and high plasticity have yet to be further developed.

Method used

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  • High-strength and high-plasticity magnesium alloy material and preparation method thereof
  • High-strength and high-plasticity magnesium alloy material and preparation method thereof
  • High-strength and high-plasticity magnesium alloy material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Purchase pure Mg, pure Zn, MgZr25 master alloy, MgNd10 master alloy, and MgGa10 master alloy with impurity content within the required range, and configure the components according to the content of the master alloy elements, as shown in Table 1.

[0033] Table 1 Ingredients weight and element content

[0034]

Zn / g

Zn / wt%

MgZr25 / g

Zr / wt%

MgNd10 / g

Nd / wt%

MgGa10 / g

Ga / wt%

Mg / g

Mg / wt%

1#

20

0.2

1200

3

3000

1

400

0.4

5380

53.8

[0035] First heat pure magnesium and pure Zn in an industrial power frequency induction melting furnace, and then pass in 1.5L / min argon gas for protection when heated to 405°C, heat to 715°C, and keep warm for 25 minutes to completely melt the metal material. After melting, keep the melt temperature at 715°C for 20 minutes, add Mg-Nd master alloy and Mg-Ga master alloy in turn, keep the melt temperature at 715°C for 12 minutes...

Embodiment 2

[0047] Purchase pure Mg, pure Zn, MgZr25 master alloy, MgNd10 master alloy, and MgGa10 master alloy with impurity content within the required range, and configure the components according to the content of the master alloy elements, as shown in Table 5.

[0048] Table 5 Ingredients weight and element content

[0049]

Zn / g

Zn / wt%

MgZr25 / g

Zr / wt%

MgNd10 / g

Nd / wt%

MgGa10 / g

Ga / wt%

Mg / g

Mg / wt%

2#

45

0.45

800

2

2000

2

800

0.8

6355

63.55

[0050] In an industrial power frequency induction melting furnace, firstly heat pure magnesium and pure Zn, and when heated to 408°C, 1.6L / min argon gas is introduced for protection, heated to 710°C, and kept for 22 minutes to completely melt the metal material. After melting, keep the melt temperature at 710°C for 20 minutes, add Mg-Nd master alloy and Mg-Ga master alloy in turn, keep the melt temperature at 710°C for 13 minu...

Embodiment 3

[0062] Purchase pure Mg, pure Zn, MgZr25 master alloy, MgNd10 master alloy, and MgGa10 master alloy with impurity content within the required range, and configure the components according to the content of the master alloy elements, as shown in Table 9.

[0063] Table 9 Ingredients Weight and Element Content

[0064]

Zn / g

Zn / wt%

MgZr25 / g

Zr / wt%

MgNd10 / g

Nd / wt%

MgGa10 / g

Ga / wt%

Mg / g

Mg / wt%

3#

95

0.95

1800

4.5

1000

3

1200

1.2

5905

59.05

[0065] First heat pure magnesium and pure Zn in an industrial power frequency induction melting furnace, and then pass in 1.6L / min argon gas for protection when heated to 408°C, heat to 705°C, and keep warm for 28 minutes to completely melt the metal material. After melting, keep the melt temperature at 705°C for 20 minutes, add Mg-Nd master alloy and Mg-Ga master alloy in turn, keep the melt temperature at 705°C for 15 mi...

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PUM

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Abstract

The present invention relates to a high-strength and high-plasticity magnesium alloy material and a preparation method thereof. The alloy material comprises the following components, by weight: 0.5-3.Swt% of Nd, 0.2-1.2wt% of Ga, 1.5 -4.5wt% of Zr, 0.1-1.0wt% of Zn; impurity elements comprising no more than 0.02wt% of Al, no more than 0.05wt% of Mn, no more than 0.01wt% of Fe, no more than 0.05wt% of Si, no more than 0.001wt% of Cu, no more than 0.001wt% of Ni and no more than 0.05v% of other impurity elements; and the balance of Mg. The preparation method comprises steps of: heating pure magnesium and pure Zn in an industrial line-frequency induction melting furnace to higher than 400 DEG C and introducing argon at 1-2.0L / min for protection; heating to 720+/-10 DEG C; insulating for 15-30 m to completely melt the metal materials; insulating for 20min after melting; successively adding a piece of Mg-Nd intermediate alloy and a piece of Mg-Ga intermediate alloy; insulating for 10-15 min after melting; adding a piece of Mg-Zr intermediate alloy; and insulating for 3-5 min after melting. The invention has the following advantages: raw materials have wide sources; and the high-strength and high-plasticity magnesium alloy material, with mechanical properties at room temperature reaching Rm no less than 350MPa and A no less than 12%, is prepared through alloying scientific formula design of Zn, Nd, Ga and Zr, and rolling and heat treatment.

Description

technical field [0001] The invention relates to a high-strength and high-plasticity magnesium alloy material and a preparation method thereof, and belongs to the technical field of non-ferrous metal alloys and preparation thereof. Background technique [0002] Magnesium alloy material is currently the lightest metal material in engineering applications, with small specific gravity, high specific strength, high specific stiffness, good electrical and thermal conductivity, good shock absorption, good electromagnetic shielding, easy cutting, easy recycling, etc. With these advantages, it is widely used in aviation, aerospace, automobiles, ships, and electronic information products, and has become the most promising metal material in the 21st century. At present, the most widely used ones are AZ91D magnesium alloy used in the foundry industry, and deformed magnesium alloys AZ31, AZ61, AZ80, ZK60 used in profiles and plates. However, the existing magnesium alloy materials have l...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C23/00C22C23/06C22C1/03C22F1/06
Inventor 刘利涛狄石磊
Owner 刘利涛
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