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Device and technique for purifying and processing titanium white waste acid

A technology for purification and treatment of titanium dioxide waste acid, which is applied in the direction of sulfur trioxide/sulfuric acid, etc., can solve the problems of difficult removal of nanometer or submicron titanium dioxide particles, high cost and impossibility, so as to reduce the burden of separation, reduce the load, The effect of increasing continuity

Inactive Publication Date: 2012-12-26
江苏江盛南节能科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the general sedimentation method is difficult to effectively remove nano or submicron titanium dioxide particles with small particle size; high-speed centrifugation method cannot be used in waste acid to remove impurity particles because of the high cost

Method used

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  • Device and technique for purifying and processing titanium white waste acid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] The structural representation of the titanium dioxide waste acid purification treatment device provided by the present invention is as follows figure 1 As shown: Titanium white waste acid purification treatment device, consists of a separation tank, a sealing cover, a clear liquid outlet, a connector, a sealing ring, a filter element, a sloping plate, a sloping plate partition, a first porous plate, a second porous plate Plate, the first support ring, the second support ring, the third support ring, the liquid outlet and the feed liquid inlet; the separation tank and the sealing cover are fixed by a sealing ring through bolts, and a clear liquid outlet is installed in the center of the top of the sealing cover. The water outlet; the upper part of the separation tank is cylindrical, the lower part is a conical structure, the conical bottom is connected with a liquid discharge port, the junction of the cylinder and the conical shape is provided with a feed liquid inlet, an...

Embodiment 2

[0019] The device structure of this embodiment is the same as that of Example 1, wherein the preferred 0.1 μm aperture of the filter core is made of polyethylene; the inclined plate material is polyethylene, and the distance between the inclined plates is 4 mm; the porous plate is polyethylene Plastic plate, the thickness of the porous plate is preferably 5cm, and the circular holes are evenly distributed on the porous plate, and the area of ​​the holes is preferably 1cm 2 , the number of holes per square meter is 2000.

[0020] Pump the titanium white waste acid solution containing powder particles into the feed liquid inlet of the device, keep the pressure at 0.05MPa, the feed liquid enters the separation tank to form a swirling flow, and some particles above the millimeter scale directly sink, containing fine The granular liquid flows through the porous plate, and first settles through the inclined plate to remove most of the particles with a size of tens of microns, and th...

Embodiment 3

[0022] The structure of the device in this embodiment is the same as in Example 1, wherein the selected filter element has a pore size of 50 μm, and the material of the filter element is ceramics; the material of the inclined plates is polypropylene, and the distance between the inclined plates is 15 mm; the porous plate is ceramics with a thickness of 1 cm plate, 30 per square meter are distributed on the perforated plate with an area of ​​200cm 2 square hole.

[0023] Pump the titanium white waste acid solution containing powder particles into the feed liquid inlet of the device, keep the pressure at 0.5 MPa, and the feed liquid enters the separation tank to form a swirling flow, and some particles above the millimeter scale directly sink, containing fine The granular liquid flows through the porous plate, and first settles through the inclined plate to remove most of the particles with a size of tens of microns, and then is further filtered through the filter element to be ...

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Abstract

The invention relates to a device and technique for purifying and processing titanium white waste acid. The device comprises a separating pot, a sealing cover, a filter core, a connector, a porous plate, supporting rings, an inclined plate and an inclined plate partition plate, wherein the separating pot and the sealing cover are fixed by a sealing ring; the sealing cover is provided with a clear solution outlet; the separating pot is of a structure with shaped cylindrical upper part and a conical lower part; the bottom of the cone is provided with a solution outlet; a material solution inlet is arranged below the cylinder; the three supporting rings are arranged from top to bottom in the separating pot; the porous plate provided with the inclined plate is arranged on the lower supporting ring; the middle supporting ring is arranged on the inclined plate and provided with the porous plate which is provided with the filter core; the upper part of the filter core is arranged on the upper supporting ring; and the water outlet of the filter core is connected with the clear solution outlet by the connector. A material solution is configured to form a rotational flow after entering the separating pot, a part of particles sink directly, the liquid flows upwards by the porous plate, a large amount of particles are settled by the inclined plate firstly, the particle impurities are removed by the filter core, the clear waste acid solution is obtained by the collection at the clear solution outlet, and the accumulated particles and powder are discharged by a solution discharge opening.

Description

technical field [0001] The invention relates to a purification device and process for waste acid solution containing powder, in particular to a purification treatment device and process for titanium white waste acid. Background technique [0002] my country is a big country in the production and consumption of titanium dioxide. At present, most enterprises in our country mainly use sulfuric acid production technology. This method produces a large amount of dilute sulfuric acid waste acid containing solid titanium dioxide particles in the production process, which is difficult to effectively utilize. The current treatment method is mainly to use distillation to concentrate waste sulfuric acid to a certain concentration and use it to realize turning waste into treasure. Among them, due to the production of titanium dioxide by the sulfuric acid method, especially when producing nano or submicron titanium dioxide products, the discharged waste sulfuric acid still contains a sma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B17/90
Inventor 李卫星付荣傅琦凤
Owner 江苏江盛南节能科技有限公司
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