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36results about How to "Mild operating temperature" patented technology

Carbon dioxide subcritical extraction, recycling and reusing method for electrolyte of waste lithium ion battery

The invention provides a carbon dioxide subcritical extraction, recycling and reusing method for the electrolyte of a waste lithium ion battery, belonging to the field of recycling and reusing of solid waste. The method comprises the following steps: after complete discharging of the waste lithium ion battery, dismounting the waste lithium ion battery and removing a shell, positive and negative terminals, sealing rings and cover plates; transferring the electrolyte, current collectors with positive and negative electrode materials and a diaphragm into a supercritical extraction apparatus; adjusting the temperature, pressure, extraction time and flow of a supercritical carbon dioxide fluid and extracting an organic solvent and an additive; and subjecting the obtained solvent to component analysis, supplementing electrolyte salt, the organic solvent and the additive according to analysis results and adjusting a ratio to prepare electrolytes with different functions. The method effectively prevents degradation and dissipation of heat-sensitive substances; operation parameters are easy to control; extraction, separation and recovery are integrated together; later complicated treating procedures are omitted; and the utilization rate of resources is higher.
Owner:HARBIN INST OF TECH

CO2 trapping method combining dimethyl carbonate absorption and membrane desorption

The invention discloses a CO2 trapping method combining dimethyl carbonate absorption and membrane desorption, belonging to the technical field of chemical engineering. The method comprises the following steps of: decarbonizing feed gas containing CO2 by dimethyl carbonate absorption; then carrying out two-stage throttling expansion and membrane desorption regeneration on CO2-absorbed absorbent rich liquor, and discharging CO2 gas generated by the throttling expansion and the membrane desorption out of the battery limit. Compared with a decarbonizing process of the inventor, which adopts the dimethyl carbonate as the absorbent, the new process of the dimethyl carbonate decarburization and the membrane desorption can reduce the comprehensive energy consumption by 5-20 percent. Compared with the propylene carbonate method maturely applied in industry at present, the energy consumption can be reduced by 30-40 percent; compared with the polyethylene glycol dimethyl ether method, the price of a solvent is lower, and polymerization losses are reduced by 40-60 percent; and compared with the low-temperature methane swabbing process, the operating temperature is milder, and the equipment investment is reduced by 30-40 percent. The CO2 removing efficiency can reach 95 percent or above.
Owner:TSINGHUA UNIV

Spent lithium-ion battery electrolyte supercritical carbon dioxide extraction process and device

The invention discloses a spent lithium-ion battery electrolyte supercritical carbon dioxide extraction process and device. The process comprises the process steps of charging, extracting and separating. A reaction kettle is changed into an up feeding and bottom discharging mode, a full-sealed conveying belt is used, up lifting and charging of a basket are omitted in charging, crushed spent lithium-ion batteries are conveyed to the top of the reaction kettle by the full-sealed conveying belt and charged, the requirement for the space height of a factory building is reduced, and safety in the production process is improved. Raffinate is sucked out and discharged by negative pressure after extraction, and production efficiency is improved. By taking the advantage of high cleaning and separating efficiency of supercritical carbon dioxide, and body poison and environmental pollution caused by residual solvents in solvent extraction are avoided. According to the process, operation temperature and pressure conditions are mild, degradation and dissipation of thermosensitive substances are effectively prevented, the recovery rate of the electrolyte is higher than 80%, and zero organic solvent discharge and high production efficiency are realized.
Owner:CAMEL GRP WUHAN OPTICS VALLEY R&D CENT CO LTD

Chemical coarsening and metallizing process for calcium magnesium titanate ceramic

The invention discloses a chemical coarsening and metallizing process for calcium magnesium titanate ceramic, belonging to the technical field of ceramic surface treatment. The invention aims to solvethe problem of poor adhesive force of a subsequent coating due to the fact that an effective coarsening process for the calcium magnesium titanate ceramic has not been reported in the industry at present. According to main points of a technical scheme in the invention, the process is characterized by specifically comprising the following steps of oil removing, roughening, adjusting, activating, peptizing, chemical copper plating and electroplating. With the process, the surface of the calcium magnesium titanate ceramic can be effectively roughened; the surface roughness of a ceramic sample before roughening is 0.4-0.5 micrometer, and the surface roughness of the sample after roughening is 0.8-1.0 micrometer, so good adhesive force is provided for a subsequent metal plating layer; technological operation is convenient, the whole process is a wet process, operation temperature is relatively mild, and risks are relatively low; and in addition, requirements on equipment are reduced, and the production cost of a product is also reduced.
Owner:麦德美科技(苏州)有限公司

Method for extracting magnesium by means of high-pressure carbonization

The invention provides a method for extracting magnesium by means of high-pressure carbonization.The method includes steps of uniformly mixing water with raw materials with magnesium to obtain reaction slurry; carrying out carbonization reaction on the reaction slurry and carbon dioxide gas under the condition of gauge pressures of 1-5 MPa to obtain serous fluid; keeping the reaction pressures and separating solid from fluid in the serous fluid to obtain fluid with heavy magnesium; reducing the pressures and decomposing the fluid with the heavy magnesium to obtain decomposed serous slurry; separating solid from fluid in the decomposed serous fluid to obtain solid and drying the solid to obtain magnesium-rich products.The method has the advantages that the method can be applied to utilizing magnesium-rich minerals such as magnesite and magnesium-rich solid waste such as boric sludge, the carbonization magnesium extraction efficiency and the calcium and magnesium separation efficiency can be improved, and energy consumption and the economic cost can be reduced to a great extent; as compared with existing processes for extracting magnesium, the method is mild in operation temperature, little in variation, low in energy consumption and heat exchange difficulty and easy to implement, required equipment is small, and the like.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Process for gasification production of synthesis gas through low temperature entrained-flow bed by using ultrafine powder

The invention discloses a process for gasification production of synthesis gas through a low temperature entrained-flow bed by using ultrafine powder. The process comprises the steps: spraying an ultrafine gasified raw material which is pulverized to less than 75 [mu]m and a gasification agent into a gasification furnace from the top of the gasification furnace of the entrained-flow bed, performing a reaction on the gasified raw material and the gasification agent so as to generate the synthesis gas containing carbon monoxide and hydrogen at a gasification temperature of lower than 1300 DEG C, spraying chilled water during downward flow of the synthesis gas, and reducing the temperature of the gas so as to meet requirements for the entrance temperature of a cyclone separator, wherein the entrance temperature of the cyclone separator is generally lower than 900 DEG C; discharging the gas with ash slag from a lower outlet of the gasification furnace after cooling, introducing the gas directly into the cyclone separator, removing most of coarse particles and a part of fine ash which are carried by the gas, then introducing the obtained gas into a waste heat boiler for further cooling of the gas, generating steam at the same time, finally introducing the gas into a filter so as to remove fine dust entrained in the gas, and sending the obtained gas to a subsequent section. In the gasification process, the ash slag does not have to reach a melt flow state, and the process is particularly suitable for production processes of low-activity coal and gasification of coal with a high-ash fusion point.
Owner:SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI

Carbon dioxide subcritical extraction and recycling method of waste lithium-ion battery electrolyte

The invention provides a carbon dioxide subcritical extraction, recycling and reusing method for the electrolyte of a waste lithium ion battery, belonging to the field of recycling and reusing of solid waste. The method comprises the following steps: after complete discharging of the waste lithium ion battery, dismounting the waste lithium ion battery and removing a shell, positive and negative terminals, sealing rings and cover plates; transferring the electrolyte, current collectors with positive and negative electrode materials and a diaphragm into a supercritical extraction apparatus; adjusting the temperature, pressure, extraction time and flow of a supercritical carbon dioxide fluid and extracting an organic solvent and an additive; and subjecting the obtained solvent to component analysis, supplementing electrolyte salt, the organic solvent and the additive according to analysis results and adjusting a ratio to prepare electrolytes with different functions. The method effectively prevents degradation and dissipation of heat-sensitive substances; operation parameters are easy to control; extraction, separation and recovery are integrated together; later complicated treating procedures are omitted; and the utilization rate of resources is higher.
Owner:HARBIN INST OF TECH

CO2 trapping method combining dimethyl carbonate absorption and membrane desorption

The invention discloses a CO2 trapping method combining dimethyl carbonate absorption and membrane desorption, belonging to the technical field of chemical engineering. The method comprises the following steps of: decarbonizing feed gas containing CO2 by dimethyl carbonate absorption; then carrying out two-stage throttling expansion and membrane desorption regeneration on CO2-absorbed absorbent rich liquor, and discharging CO2 gas generated by the throttling expansion and the membrane desorption out of the battery limit. Compared with a decarbonizing process of the inventor, which adopts the dimethyl carbonate as the absorbent, the new process of the dimethyl carbonate decarburization and the membrane desorption can reduce the comprehensive energy consumption by 5-20 percent. Compared with the propylene carbonate method maturely applied in industry at present, the energy consumption can be reduced by 30-40 percent; compared with the polyethylene glycol dimethyl ether method, the priceof a solvent is lower, and polymerization losses are reduced by 40-60 percent; and compared with the low-temperature methane swabbing process, the operating temperature is milder, and the equipment investment is reduced by 30-40 percent. The CO2 removing efficiency can reach 95 percent or above.
Owner:TSINGHUA UNIV

A humidifying-dehumidifying seawater or brackish water desalination device and method

The present invention belongs to a humidification-dehumidification desalination method and apparatus for sea water or brackish water, and the apparatus includes pretreatment system and a humidification-dehumidification system. The pretreated seawater or brackish water is introduced into a storage tank, preheated by a heater, pumped into a humidification tower; and then the seawater or brackish water passes through an overhead liquid distributor and directly contacts with the bottom-up carrier gas flowing through a packed column, so as to humidify the carrier gas; and the carrier gas with high humidity is introduced to dehumidification tower bottom via a pipeline, and direct contacts with the top-down cooling water, and the water vapor is condensed and discharged with cooling water, so as to obtain fresh water. The method uses the characteristics of large specific surface area and small resistance of the filler, realizes gas-liquid interphase faster heat and mass transfer, and is applicable to sea island, desert and thermal power plants. Compared with the prior desalination technology, the apparatus has the characteristics of simple equipment, easy operation, easy treatment and cleaning, small investment, and easy operation and maintenance.
Owner:ZHEJIANG UNIV

A kind of method for extracting magnesium by high-pressure carbonization

The invention provides a method for extracting magnesium by means of high-pressure carbonization.The method includes steps of uniformly mixing water with raw materials with magnesium to obtain reaction slurry; carrying out carbonization reaction on the reaction slurry and carbon dioxide gas under the condition of gauge pressures of 1-5 MPa to obtain serous fluid; keeping the reaction pressures and separating solid from fluid in the serous fluid to obtain fluid with heavy magnesium; reducing the pressures and decomposing the fluid with the heavy magnesium to obtain decomposed serous slurry; separating solid from fluid in the decomposed serous fluid to obtain solid and drying the solid to obtain magnesium-rich products.The method has the advantages that the method can be applied to utilizing magnesium-rich minerals such as magnesite and magnesium-rich solid waste such as boric sludge, the carbonization magnesium extraction efficiency and the calcium and magnesium separation efficiency can be improved, and energy consumption and the economic cost can be reduced to a great extent; as compared with existing processes for extracting magnesium, the method is mild in operation temperature, little in variation, low in energy consumption and heat exchange difficulty and easy to implement, required equipment is small, and the like.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI
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