66 results about "Callicarpa" patented technology

The invention discloses a vacuum freeze-drying process of callicarpa leaf and a preparation process of callicarpa leaf powder. The vacuum freeze-drying process of the callicarpa leaf comprises the following steps: (1) selecting raw materials; (2) cleaning: quickly leaching the callicarpa leaf; (3) pre-drying: pre-drying the callicarpa leaf till water content is 60-70%; (4) loading onto a plate and pre-freezing: loading the pre-dried callicarpa leaf onto the plate, and gradually cooling for 2-3 hours, and then pre-freezing at the temperature of (-20)-(-40) DEG C, wherein the loading weigh is 2.7-4 kg/m<2> and the loading thickness is 2-3 cm; (5) sublimation drying: vacuumizing until the absolute pressure of the system is 100 Pa, entering a heating process, raising the shed temperature to 40-70 DEG C while controlling the vacuum degree at 55-65 Pa, and carrying out sublimation drying for 10-15 hours; and (6) desorption drying: maintaining the material temperature at 20-50 DEG C and discharging when the water content is below 3%. In the vacuum freeze-drying process of the callicarpa leaf disclosed by the invention, the vacuum freezing time, temperature, pressure and other parameters are reasonably set, so that the pharmaceutically active ingredients are maximally maintained.

The invention discloses a traditional Chinese medicine preparation used for treating gastric ulcer and a preparation method, and belongs to the field of traditional Chinese medicine. The effective components of the traditional Chinese medicine preparation comprise the following raw materials: limonium sinense, water caltrop pedicle, rumex nepalensis spreng, callicarpa, Japanese clover, common tree roots, buckbean, himalayan eriosema roots, ilex rotunda thunb, immature fruits of cassia bark trees, roots of rock cotoneaster, lignum dalbergiae odoriferae, wrinkled gianthyssop herbs, cydonia oblonga, chalk and asarum forbesii maxim. Compatibility of drugs of the traditional Chinese medicine preparation is good, and the traditional Chinese medicine preparation has double functions of treatment and conditioning; the drugs are compatible to endow the traditional Chinese medicine preparation with the effects of promoting qi circulation to relieve pain, invigorating spleen to promote design, tranquilizing mind by nourishing the heart, promoting blood circulation and arresting bleeding and the like, thereby having a good curative effect on patients suffering from gastric ulcer; the traditional Chinese medicine preparation has the advantages that the traditional Chinese medicine preparation is easy and convenient to prepare, works quickly and can fundamentally treat gastric ulcer, medicinal herb resources are abundant and the cost is low, so that the traditional Chinese medicine preparation can be widely used and popularized clinically.

The invention discloses a medicinal composition for treating burn and scald. The medicinal composition comprises the following bulk drugs in percentage by weight: 13 percent of garden burnet, 10 percent of rhizoma bletillae, 10 percent of callicarpa undiflora, 27 percent of rhubarb, 15 percent of giant knotweed, 10 percent of barbed skullcap herb and 15 percent of gromwell root, wherein the medicaments are settled and crushed into fine powder and then uniformly mixed to obtain a mixture; the mixture is immersed in sesame oil in a ratio of 1:(6-8) to obtain a second mixture; and the second mixture is sieved to filter off residues and is bottled for later use. The medicinal composition has the advantages of powerful anti-infection, pain relieving and impervious functions, no irritation to a wound surface, capability of promoting repairing and healing of the wound surface of a cut, locally flat healed wound surface, no scar on the healed wound surface of the first, second and third degree burns and scalds, short treatment period, no irritation phenomenon, no toxic or side effect, low treatment cost, convenience in operation, easiness in change of a medical prescription and convenience in nursing. The medicinal composition can be used for reducing and treating hypertrophic scar of deep second degree burn and superficial third degree burn, promoting the healing of the wound surface and is an external pure traditional Chinese medicine for treating the burn and scald without being limit by medical conditions during operation and implementation.

The invention discloses a Chinese medicinal herb for treating contact dermatitis. The Chinese medicinal herb is prepared from the following medicaments in parts by weight: 30-40 parts of skunk bugbane, 30-40 parts of Chinese angelica, 20-30 parts of honeysuckle flower, 20-30 parts of red paeony root, 15-25 parts of weeping forsythia, 20-30 parts of burdock seed, 20-30 parts of notopterygium root, 20-30 parts of divaricate saposhnikovia root, 20-30 parts of dahurian angelica root, 20-30 parts of safflower, 20-30 parts of talc, 20-30 parts of dandelion, 10-20 parts of ford nervilia leaf, 20-30 parts of rosidae root, 15-25 parts of callicarpa undiflora and 20-30 parts of Chinese ladiestresses rootor herb. In the formula, skunk bugbane serves as chief medicinal; Chinese angelica and honeysuckle flower serve as deputy medicinal; red paeony root, weeping forsythia, burdock seed, notopterygium root and divaricate saposhnikovia root serve as assistant medicinal; and dahurian angelica root, safflower, talc, dandelion, ford nervilia leaf, rosidae root, callicarpa undiflora and Chinese ladiestresses rootor herb serve as envoy medicinal. The Chinese medicinal herb is convenient to prepare and use, is safe, has no side effect, has low treatment cost, and is an ideal medicament for treating contact dermatitis.

The invention discloses an artificial cross breeding method for a callicarpa eucallicarpa plant. The method comprises choosing male parent inflorescence one day prior to flowering to perform bagging and collect pollen one day prior to cross breeding, at 10 to 11 on the morning of a sunny day at a full-bloom stage of July; choosing female parent inflorescence one day prior to flowering on the day of cross breeding to perform castration, continuously performing pollination twice on the same day and next day, and performing bagging; and removing bags 15 days after pollination, enabling mesh bags to be sleeved on fruits on November to avoid fruit abscission, harvesting the fruits on December, stripping out seeds, and storing the seeds below 4 DEG C. According to the artificial cross breeding method, cross breeding efficiency and fruit set percentage are effectively improved, more cross breeding progeny can be obtained, and garden seed breeding of the callicarpa plant is promoted.

The invention discloses a method for extracting total phenylpropanoid glycosides from Guangdong Zizhu, which is characterized in that: Guangdong Zizhu medicinal material is cut into sections, added with 5-10 times the amount of aqueous solution for microwave extraction for 2-3 times, and the extract is used for filtering Ultrafiltration membrane ultrafiltration, the collected permeate is added to the nanofiltration membrane system for concentration, the collected concentrated solution is added to the activated carbon column for adsorption, ethanol solution gradient elution, the target components are collected, concentrated and dried under reduced pressure to obtain the total phenylpropanoid glycosides. The method of the invention has the advantages of simple operation, high extraction rate, low energy consumption, little pollution and easy industrial production.

The invention discloses a medicinal hemostatic. The hemostatic is prepared from 25 Chinese herbal medicines in parts by weight: 3 to 5 parts of common cephalanoplos herb, 3 to 5 parts of panax pseudoginseng, 3 to 5 parts of mugwort leaf, 3 to 5 parts of hairyvein agrimony, 3 to 5 parts of radix callicarpa, 1 to 3 parts of imperata cylindrical, 1 to 3 parts of cicada slough, 2 to 4 parts of rhizoma arisaematis, and the like. Compared with the prior art, the hemostatic has convenient use and low cost by using the technical solution, and greatly improves hemostatic effect; the affected part heals completely without operation, and is free of other complications. The hemostatic not only is used before operation, such as the trauma, but also is used after operation, such as the cut caused by the operation; since applicable range is wide, the hemostatic is not only applicable for hospital, but also applicable for family, journey, and the places which are easy to injure, such as battlefield, playground.

The invention discloses a drug for treating puerperium haemorrhage. The drug comprises the following components: 10 parts-30 parts of pseudo-ginseng, 30 parts-50 parts of Chinese angelica, 10 parts-30 parts of peach seeds, 10 parts-30 parts of bupleurum, 10 parts-30 parts of stigma croci, 5 parts-15 parts of Yunnan white powder, 10 parts-30 parts of hairyvein agrimony, 10 parts-30 parts of bletilla, 10 parts-15 parts of callicarpa undiflora and the like, wherein the pseudo-ginseng, the Chinese angelica, the peach seeds, the Yunnan white powder, the callicarpa undiflora and the like are main drugs. The pseudo-ginseng, the Chinese angelica, the peach seeds, the Yunnan white powder, the callicarpa undiflora and the like have the functions of hemostasis, antibiosis, diminishing inflammation and replenishing blood, can effectively stop bleeding to prevent a puerpera from shocking or threat to life caused by losing the blood too much, and can have the functions of antisepsis, anti-inflammation and preventing infection and a complication from causing. In addition, the pseudo-ginseng, the Chinese angelica, the peach seeds, the Yunnan white powder, the callicarpa undiflora and the like can replenish the blood effectively, and improve the habitus and an immunity of a patient. Not only can the disease be promoted to recover, but also the quality of milk can be guaranteed. The patient and an infant can both receive the benefit. The other Chinese herbal medicinal ingredients can not only guarantee respective pesticide effect after being manufactured to be apozem, but also supplement each other and take advantages from each other. The state of an illness of bleeding can be effectively suppressed, and the recovery of the state of the illness is promoted.

A method for repelling arthropods involving treating a subject or an object with an arthropod repelling composition containing an arthropod repelling effective amount of at least one clerodane of the formula

in which R¹ is H, halogen, formyl, a straight chain or branched C_1-4 saturated alkyl, a straight chain or branched C_2-4 unsaturated alkyl, or an aryl containing 6-10 carbon atoms in the ring skeleton thereof, wherein R¹ is unsubstituted or substituted with one or more substituents, which are the same or different, selected from the group consisting of oxo (═O), OR², CO₂R², and OC(O)R², wherein R² is H, a straight chain or branched C_1-30 saturated alkyl, a straight chain or branched C_2-30 unsaturated alkyl, or an aryl comprising 6-10 carbon atoms in the ring skeleton thereof; wherein R² is unsubstituted or substituted with one or more substituents selected from the group consisting of halogen, amino, hydroxyl, oxo (═O), thio, cyano and nitro; optionally a carrier, optionally an arthropod repellant, and optionally an insecticide. Preferably the compound is 13,14,15,16-tetranorclerod-3-en-12-al (callicarpenal), 13,14,15,16-tetranorclerod-3-en-12-ol, 13,14,15,16-tetranorclerod-3-en-12-oic acid, β-epoxycallicarpenal, α-epoxycallicarpenal, or mixtures thereof. Also a compound of the above formula. Also an arthropod repellant composition containing an arthropod repelling effective amount of at least one of the compounds of the above formula and a carrier. The present invention does not involve the use of any compound isolated from Callicarpa species other than callicarpenal, intermedeol, or spathulenol.

The invention relates to a biopreparation for poisoning pine nematodes and its preparing method and application. Its producing bacterial strain-Caryospora callicarpa ZD2 has a preserved number of CGMCC NO.0983. After fermented by liquid and solid, the ZD2 bacterial strain is prepared into a biopreparation with poisoning activity for pine nematodes. The invention has a good poisoning effect on the pine nematodes and a good prospect in application and development.

The invention discloses a traditional Chinese medicinal preparation for curing upper gastrointestinal hemorrhage. Selected raw medicines comprise 10-20g of Callicarpa undiflora, 10-20g of bletilla striata, 10-20g of garden burnet, 10-20g of hedgehog hide, 5-10g of fried cattail pollen, 8-12g of radix notoginseng, 8-15g of flying squirrel feces, 10-20g of medicated leaven, 8-12g of coptis, 5-10g of dark plum, 10-20g of fructus amomi, 8-12g of calcined Longmu,8-12g of Chinese gall, 8-12g of aspongopus, 10-20g of donkey-hide gelatin, 8-12g of Agrimonia pilosa Ldb., 8-12g of gentrin knotweed and 8-12g of charcoal of ginger. By compatibility of above medicines, the traditional Chinese medicinal preparation has effects of restraining ulcer, stopping bleeding, removing stasis, relieving pain, removing blood stasis to promote tissue regeneration, tonifying qi, cooling blood, relieving hyperacidity, engendering flesh and the like. The traditional Chinese medicinal preparation is used for curing upper gastrointestinal hemorrhage, has advantages of fast effectiveness, short treatment course, no side-effect and high cure rate, and is worth of clinic popularization and application.

The present invention relates to the field of pesticides, in particular to a composition for controlling botrytis cinerea of broccoli, which comprises the following raw materials in parts by weight: 10 to 20 parts of callicarpa bodinieri, 12 to 18 parts of gentiana macrophylla, 12 to 18 parts of Herba Pteridis multifidae, 2 to 8 parts of radix semiaquilegiae, 12 to 18 parts of commelina communis,10 to 20 parts of manyleaf paris rhizome, 12 to 18 parts of Belamcanda sinensis, 2 to 8 parts of Flos Eriocauli, 10-20 parts of Chinese holly, 12-18 parts of tobacco, 8-12 parts of fructus piperis longi, 8-12 parts of polygonum cuspidatum, 3-9 parts of fructus trichosanthis, 8-12 parts of reed rhizome, 6-8 parts of complex bacteria, 10-20 parts of complex amino acid, and 8-12 parts of multi-vitamin. The composition of the invention cannot cause harm to the broccoli, and at the same time, the composition has the good prevention and control effect on the botrytis cinerea of broccoli, the incidence of the botrytis cinerea of broccoli is controlled at 1.23%, the total effective rate of the broccoli infected with botrytis cinerea is more than 95%, and the control effect is remarkable.

The invention relates to a pure Chinese medicinal composition for treating infectious hemorrhagic disease of grass carp and a preparation method thereof. The composition is prepared by mixing the following components in part by weight: 15 to 35 parts of hairyvein agrimonia herb and bud, 15 to 35 parts of callicarpa undiflora, 15 to 35 parts of isatis root, 25 to 45 parts of rhubarb, 25 to 45 parts of dried orange peel, 15 to 35 parts of lightyellow sophora root, 20 to 40 parts of Chinese pulsatilla root and 20 to 40 parts of sweet wormwood herb. The pure Chinese medicinal composition is reasonable in formula, is easy to prepare, does not have any toxic or side effect, is subjected to superfine grinding, is high in bioavailability, treats both symptoms and root causes, has a very obvious curative effect and is clinically proven to have a special effect of treating infectious hemorrhagic disease of grass carp, and medicine residue and medicine resistance are avoided.

The invention discloses air-dried beef prepared from fingered citron and a processing method of the air-dried beef. The air-dried beef is prepared from the following raw materials in parts by weight: 80-100 parts of beef, 4-6 parts of fingered citron, 2-3 parts of flosmume, 2-4 parts of radix polygoni multiflori, 1-3 parts of parasitic loranthus, 2-4 parts of cattail pollen, 1-3 parts of rhizoma polygonati, 2-3 parts of radix puerariae, 1-3 parts of fructus corni, 2-4 parts of rhizoma alismatis, 1-3 parts of callicarpa undiflora, 8-10 parts of white spirit, 1-2 parts of aginomoto, 5-7 parts of salt, and 6-8 parts of a nutrition additive. The invention discloses the air-dried beef prepared from fingered citron. The processing method is simple to operate and reasonable in formula. The air-dried beef produced by the processing method has the characteristics of dry and comfortable texture, moderate hardness, no cowy, and sweet and good taste, has a little faint scent of fingered citron, and is a good leisure food with a health-care effect.

The invention discloses a method for preparing high-purity poliumoside. The method comprises the following steps of: smashing callicarpa kwangtungensis serving as a medicinal material; adding a 50-70 percent acetone solution in an amount which is 5-7 times that of the medicinal material for performing ultrasonic extraction for 2-3 times; filtering the extracting solution to recover a solvent; adding a concentrated solution into water-saturated n-butyl alcohol for extracting; making the extraction liquid pass through a short aluminum oxide column; recovering a reagent from the column passing liquid; separating the obtained extract by adopting a high-speed counter-flow chromatography; detecting with an ultraviolet detector; collecting a target component; and drying under reduced pressure to obtain a poliumoside monomer. The method for preparing the high-purity poliumoside has simple process steps, large preparation amount and a short period, and the purity of the obtained product is not less than 98 percent.

The invention relates to the technical field of pesticides and discloses a biogenic pesticide. The biogenic pesticide comprises the following components by weight: 10-14 parts of inspect repelling vernonia esculenta, 15-21 parts of camphor tree, 22-26 parts of ajuga decumbens thunb, 13-18 parts of needle juniper, 16-20 parts of cuculus canorus, 15-18 parts of callicarpa longissimi, 17-21 parts ofartemisia apiacea, 19-25 parts of gelsemium elegan, and 8-12 parts of a biological bacterium agent. The pesticide effect of the biogenic pesticide is strong and lasts long, the biogenic pesticide is an organic pesticide, the toxic ingredients are extracted from the plants, the pesticide residue is naturally degraded after the pesticide is sprayed on the crop and the plant diseases and insect pestsare killed, and the biogenic pesticide is environmentally friendly.