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184results about How to "Increase the rate of hydrolysis" patented technology

Short-chain volatile fatty acid and preparation method thereof

The invention discloses a short-chain volatile fatty acid and a preparation method thereof. The preparation method for the short-chain volatile fatty acid comprises the following steps of employing sludge as a fermentation substrate; adding sodium nitrite into the fermentation substrate, performing pretreatment in an acid environment, and performing anaerobic fermentation under an alkaline condition to obtain the short-chain volatile fatty acid. According to the short-chain volatile fatty acid and the preparation method thereof, the sludge of a sewage treatment plant is taken as a raw material, and is jointly treated by virtue of free nitrite pretreatment and alkaline anaerobic fermentation, and the concentration of free nitrite in the system, the pretreatment time, the fermentation pH value and the action of microorganisms in the sludge are controlled to maximally convert undissolved sludge organic matters in the sludge into the short-chain volatile fatty acid, so that the yield of the volatile fatty acid produced from the sludge is further increased on the basis of resourcefully utilizing the sludge and reducing environmental pollution caused by the sludge, and the reaction time is shortened; the short-chain volatile fatty acid and the preparation method thereof have the advantages of high product yield, simple preparation method, energy conservation, consumption reduction, low running cost and the like.
Owner:HUNAN UNIV

Method for extracting rapeseed peptides through wet milling combined with enzymic method

The invention discloses a method for extracting rapeseed peptides through wet milling combined with an enzymic method. The method comprises the following steps of: taking dry degreased and unshelled rapeseed dregs, grinding and filtering the dry degreased and unshelled rapeseed dregs through a 40-mesh sieve, adding water which is 5 times of the materials in weight, adding 5-10 u / g of cellulase, and performing wet grinding on black soybean meal for 1-3 hours under the condition of a rotating speed in the range from 250 to 400 rpm (revolutions per minute) by using a ball mill to obtain an ultrathin powder turbid liquid; (2) supplementing water to the ultrathin powder turbid liquid until the concentration of the dry materials is in the range from 50 to 100 g / l, adjusting the pH to 7.0, adding 40u / g of protease, maintaining the temperature at 55 DEG C and the pH at 7.0, and hydrolyzing for 1-2 hours; (3) centrifuging the enzymatic hydrolysate for 15 minutes under the condition of 10000 rpm, continuously adding water which is 5-10 times of residues in weight to the residues, adding 20u / g of protease, hydrolyzing for 1-2 hours at the temperature of 55 DEG C and the pH of 7.0, centrifuging, and blending the two supernates to obtain a rough peptide solution. According to the invention, cellulose dissolving causes large-molecular materials such as protein to be hydrolyzed more easily, and also the hydrolysis rate of the protein can be increased; in addition, the conversion rate of the peptides is greatly increased.
Owner:ZHENJIANG AGRI SCI INST JIANGSU HILLY AREAS

Method for preparing mesoporous silica spherical nanoparticles

InactiveCN107381579ALow costFacilitate macro quantization synthesisSilicaNanotechnologyTetraethyl orthosilicateNanoparticle
The invention discloses a method for preparing mesoporous silica spherical nanoparticles. According to the method, the used template agent refers to cetyl trimethyl ammonium bromide, the alkali source refers to an organic small molecule amine, the silicon source refers to tetraethyl orthosilicate (TEOS), and the organic alcohol salt serves as a promoter. According to the molar composition of the raw materials, a ratio of the silicon source to the cetyl trimethyl ammonium bromide to organic alkali to sodium methylate to water is (1):(0.03-00.06):(0.5-2):(0.001-0.5):(80-500). Accurate synthesis in the particle size range of 25-50nm is realized by regulating the amount of the organic alcohol salt and regulating the nucleation rate of particles. Compared with the prior art, the method disclosed by the invention has the most significant advantage that the hydrolysis and condensation rate of the silicon source is promoted by taking the organic alcohol salt with high nucleophilicity as the promoter. Therefore, the silicon source is subjected to burst nucleation in a very short time, so that the small-size mesoporous silica spherical nanoparticles are prepared. The synthetic method disclosed by the invention is simple, short in cycle, low in cost and high in repeatability and is an environment-friendly green synthetic method.
Owner:EAST CHINA NORMAL UNIVERSITY

Aluminum-based composite hydrogen manufacturing material and preparation method thereof

The invention provides an aluminum-based composite hydrogen manufacturing material and a preparation method thereof and belongs to the technical field of energy sources. The invention provides a novel aluminum-based composite material with high hydrogen manufacturing velocity, and the novel aluminum-based composite material is manufactured by a mechanical ball milling method; and different aluminum-based raw materials and additives are selected in the manufacturing process, and the reaction activity of products and water is improved by optimizing the content of each component and ball millingconditions. The aluminum-based composite hydrogen manufacturing material manufactured by the preparation method provided by the invention can quickly react with the water to release hydrogen at normal temperature, the initial hydrogen manufacturing velocity is larger than 2,000ml/g.min, and the hydrogen yield is close to a theoretical value. The aluminum-based composite hydrogen manufacturing material can be used for solving the problem of low hydrogen manufacturing velocity at the normal temperature reported at present, the hydrogen manufacturing method is simple and fast, and the products are portable and can supply hydrogen to fuel batteries, movable devices and the like.
Owner:LIAONING NORMAL UNIVERSITY

Preparation method of hybrid hydrolase formulation for promoting methane yield from fermentation

InactiveCN1884509AIncrease fermentation gas productionPromote degradationHydrolasesMicroorganismsBiotechnologyMethane yield
The method for preparation of hydrolytic enzyme preparation used for improving gas-producing rate of marsh gas fermentation belongs to preparation of supplementary exoenzyme used for marsh gas fermentation. The invention is to provide a method for preparation of hydrolytic enzyme preparation used for improving gas-producing rate of marsh gas fermentation, which has the production bacteria with the following enzymatic vitality index: selecting wheat bran and rice bran as mixed culture medium, obtaining mixed bran seeds by pedigree breed two-stage enlargement culture of the bacteria with solid method, fermenting for 3-4 days at 28 DEG after evenly mixed, sampling and analyzing every enzymatic vitality index, adding commodity enzyme preparation to reach enzymatic vitality index, and airing until the humidity is lower than 5%. The enzymatic vitality index of the prolease in the said mixed bran seeds is not more than 2000+-5% mug tyrosine / g / min. The bacteria can be obtained by bacteria and fungus separated from different environment. The test proves that when hydrolytic enzyme preparation is input into the methane tank fermentation raw materials, the rate of dissolution and degradation of the marsh gas fermentation raw materials can be improve, and the gas-producing rate of marsh gas fermentation, TS and VS gas-production potential and methane content in marsh gas can be increased.
Owner:YUNNAN NORMAL UNIV

Joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime

The invention discloses a joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime. The material comprises the steps that reaction liquid obtained by raw materials through an ammoximation reaction and a hydrooximation reaction is extracted and separated to obtain an organic phase, the organic phase is prepared into product cyclohexanone-oxime, or part of the organic phase and part of product cyclohexanone-oxime are adopted as raw materials for an oxime hydrolysis reaction to be hydrolyzed, the organic phase in hydrolysis liquid is circulated to return to a oximation reactor, part of an inorganic phase in the hydrolysis liquid is adopted as a raw material to be circulated to return to a hydroxylamine oximation reactor, and the other part of the inorganic phase is prepared into a hydroxylamine aqueous solution and hydroxylammonium salt. The joint production technology of hydroxylamine, hydroxylammonium salt and cyclohexanone-oxime is simple in procedure, the requirement of the ammoximation reaction for the purity of the raw material cyclohexanone and the catalyst performance is lowered, a high quality cyclohexanone-oxime product without cyclohexanone is obtained, the simplification of the downstream caprolactam technology and the improvement of the product quality are benefited, and the hydroxylamine and hydroxylammonium salt product which have high additional value are obtained simultaneously.
Owner:河北美邦工程科技股份有限公司
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