Zhenlong xingnao (Chinese character) capsule of Tibetan medicine composition and detection method of iron content in preparation thereof
A quality inspection method, Zhenlong Xinnao technology, applied in capsule delivery, pharmaceutical formula, plant raw materials, etc.
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Embodiment 1
[0060] Example 1: Determination of Iron Content in Zhenlong Xingnao Capsules
[0061] Zhenlong Xingnao Capsules include TLC identification of saffron, TLC identification of pearls, TLC identification of cholic acid, TLC identification of cinnamon aldehyde, and content determination items of cinnamon aldehyde, (also available These measurements are not included), and the following measurements are also included:
[0062] Take 8g of the content powder of the Tibetan medicine composition Zhenlong Xinnao Capsule, weigh it accurately, put the crucible containing the sample on the electric furnace and burn it slowly (to avoid burning, swelling, overflowing), until the test sample is completely carbonized, It was black and no longer smoked, and was allowed to cool to room temperature. Add an appropriate amount of 2ml of sulfuric acid dropwise to make the charcoal completely wet, continue to heat until the steam is removed and the white smoke is exhausted, blaze at 600°C for 4 hours,...
Embodiment 2
[0064] Embodiment 2: Determination of iron content in Zhenlong Xingnao Granules
[0065] Zhenlong Xingnao Granules include TLC identification of saffron, TLC identification of pearls, TLC identification of cholic acid, TLC identification of cinnamon aldehyde, and content determination items of cinnamon aldehyde, (also available These measurements are not included), and the following measurements are also included:
[0066]Take 7g of Zhenlong Xingnao granule powder, a Tibetan medicine composition, and weigh it accurately. Put the crucible containing the sample on the electric furnace and burn it slowly (avoid burning, swelling, overflowing), until the test sample is completely carbonized and black , and no longer smoke, let cool to room temperature. Add an appropriate amount of 1ml of sulfuric acid dropwise to make the charcoal completely wet, continue to heat until the steam is removed and the white smoke is exhausted, blaze at 550°C for 5 hours, let cool, wash with 50ml of c...
Embodiment 3
[0069] Example 3: Determination of Iron Content in Zhenlong Xingnao Pills
[0070] Zhenlong Xingnao Pills include TLC identification of saffron, TLC identification of pearls, TLC identification of cholic acid, TLC identification of cinnamon aldehyde, and content determination items of cinnamon aldehyde, (also available These measurements are not included), and the following measurements are also included:
[0071] Take 8g of Zhenlong Xingnao Pill powder, a Tibetan medicine composition, and weigh it accurately. Put the crucible containing the sample on the electric furnace and burn it slowly (avoid burning, swelling, overflowing), until the test sample is completely carbonized and black , and no longer smoke, let cool to room temperature. Add an appropriate amount of 2ml of sulfuric acid dropwise to make the charcoal completely wet, continue to heat until the steam is removed and the white smoke is exhausted, blaze at 550°C for 4 hours, let cool, wash with 50ml of concentrated...
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