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Low-temperature rolling method for preparing molybdenum-copper alloy

A technology of molybdenum-copper alloy and rolling speed, which is applied in the direction of metal rolling, can solve the problems of low processing efficiency, poor processing accuracy, and large equipment investment, and achieve high production efficiency, improved material utilization rate, and low equipment investment. Effect

Active Publication Date: 2014-11-12
上海瑞钼特科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The purpose of the present invention is to provide a low-temperature rolling method for preparing molybdenum-copper alloy, which solves the problems of large equipment investment, poor processing precision, low processing efficiency and low material utilization rate in the existing production process of molybdenum-copper alloy foil. The processing accuracy and production efficiency of molybdenum-copper alloy foil are improved, and the method of preheating and heat preservation further reduces the number of rolling passes and improves production efficiency

Method used

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  • Low-temperature rolling method for preparing molybdenum-copper alloy

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Effect test

Embodiment 1

[0042] A molybdenum-copper alloy sintered blank with a weight percentage of 20% copper and 80% molybdenum is obtained by powder rolling process, and its thickness is 0.5mm; The alloy billet is preheated to 40-100°C in an oven, and the heat preservation time is 5-8min; then the preheated molybdenum-copper alloy billet is quickly rolled directly on a twenty-roller plate rolling mill, and the processing amount per pass is less than or equal to 45%. The rolling speed is 8m / s; when the processing volume of the pass is reached, the molybdenum-copper alloy billet is quickly put into the oven and kept at a temperature of 40-100°C for 5-8min, and then rolled again; so after 3 passes Rolling can produce a molybdenum-copper alloy foil with a thickness of 0.25mm. After measurement, the density of the molybdenum-copper alloy foil can reach 99.95%, the thickness tolerance is 3 microns, the surface roughness is Ra0.05, and the input-output ratio reaches 89%.

Embodiment 2

[0044] A molybdenum-copper alloy sintered blank with a weight percentage of 25% copper and 75% molybdenum is prepared by powder molding process, and its thickness is 1.5mm; the rolls of the two-roll plate mill are preheated to 40-80°C; the molybdenum-copper alloy blank is Preheat in an oven to 40-90°C, keep warm for 10-15min; then quickly roll the preheated molybdenum-copper alloy billet directly on a two-roll plate rolling mill, the processing amount per pass is less than or equal to 45%, and the rolling speed It is 15m / s; when the processing volume of each pass is reached, the molybdenum-copper alloy billet is quickly put into the oven at a temperature of 40-90°C for another 10-15min, and then rolled again; after 5 passes of rolling, A molybdenum-copper alloy foil with a thickness of 0.05 mm can be obtained. After measurement, the density of the molybdenum-copper alloy foil can reach 99.95%, the thickness tolerance is 3 microns, the surface roughness is Ra0.05, and the input...

Embodiment 3

[0046] A molybdenum-copper alloy sintered blank with a weight percentage of 20% copper and 80% molybdenum is obtained by powder rolling process, and its thickness is 0.5mm; The alloy billet is preheated to 40-100°C in an oven, and the heat preservation time is 5-8min; then the preheated molybdenum-copper alloy billet is quickly rolled directly on a twenty-roller plate rolling mill, and the processing amount per pass is less than or equal to 55%. The rolling speed is 8m / s; when the processing volume of each pass is reached, the molybdenum-copper alloy billet is quickly put into the oven at a temperature of 150-260°C for another 5-8min, and then rolled again; so after 2 passes Rolling can produce a molybdenum-copper alloy foil with a thickness of 0.05mm. After measurement, the density of the molybdenum-copper alloy foil can reach 99.5%, the thickness tolerance is 3 microns, the surface roughness is Ra0.05, and the input-output ratio reaches 85%.

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Abstract

The invention discloses a method for preparing molybdenum-copper foil, which includes the steps of: (1) preparing sintered molybdenum-copper billet through a normal method; (2) preheating the molybdenum-copper billet to 40-300DEG C, thermally insulating the billet for 5-30mins for standby use; (3) preheating a roller of a rolling mill to 40-80DEG C; and (4) rolling the preheated molybdenum-copper billet on the rolling mill to obtain the molybdenum-copper foil. By adopting a low-temperature rolling method, the invention overcomes the problems of big equipment investment, poor machining precision and low material utilization ratio in the prior production process. The method improves the machining precision and the production efficiency of the molybdenum-copper foil.

Description

technical field [0001] The invention belongs to the field of preparing molybdenum-copper alloys, in particular to a low-temperature rolling method for preparing molybdenum-copper alloys. Background technique [0002] Molybdenum-copper alloy is a pseudo-alloy material composed of molybdenum and copper elements. Because of its low expansion coefficient and good electrical and thermal conductivity, it has been widely used in electrical components, semiconductor packaging, electronics and other industries. In recent years It has also been valued in the high-power LED lighting chip industry and has a large potential market. However, molybdenum-copper alloy foil parts used in the semiconductor packaging industry, electronics and high-power LED lighting industries generally require greater than 99.5% of the theoretical density due to the high density; the thickness is thin, generally 80-200 microns, and the thickness tolerance It is required to be within 5 microns, and the surface...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B21B3/00
Inventor 王涛
Owner 上海瑞钼特科技股份有限公司