Shear thickening fluid based on molecular colloid and preparation method and application of shear thickening fluid
A technology of molecular colloids and fluids, applied in chemical instruments and methods, textiles and papermaking, compounds of Group 4/14 elements of the periodic table, etc. Less problems, to achieve the effect of low cost, simple process and preventing agglomeration
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Embodiment 1
[0041] Preparation of PBDMS (filled with nano-silica) molecular colloid:
[0042] (1) Weigh nano-silica, boric acid and hydroxy silicone oil with a mass ratio of 1:1:10, of which hydroxy silicone oil (Zhonghao Chenguang Chemical Research Institute, brand GY-209-3, polymerization degree 3-5 ) is 350g, boric acid and nano silicon dioxide (Degussa Silica Co., Ltd., the trade mark is VN 3 ) have a mass of 35g respectively. First, add nano silicon dioxide into hydroxy silicone oil, stir at a high speed (1000rpm / min), after the nanoparticles are evenly distributed in hydroxy silicone oil, then add boric acid particles, put them in a beaker and stir fully, the stirring time is 0.5h;
[0043] (2) Pour the above-mentioned suspension dispersion system into an aluminum pan, and then place the aluminum pan on a heating plate with a constant temperature of 300°C. The mixed liquid in no longer flows;
[0044] (3) After the reaction was completed, the material in the aluminum plate was co...
Embodiment 2
[0047] Preparation of PBDMS (filled with nano-montmorillonite) molecular colloid:
[0048] (1) Weigh nanometer montmorillonite, boric acid and hydroxy silicone oil with a mass ratio of 1:1:10, among which hydroxy silicone oil (Zhonghao Chenguang Chemical Research Institute, brand GY-209-3, polymerization degree 3-5 ) is 350g, boric acid and nano-montmorillonite (Zhejiang Fenghong New Material Co., Ltd., the trade mark is DK 1 ) have a mass of 35g respectively. Add the nano-montmorillonite into the hydroxyl silicone oil, stir at a high speed (1000rpm / min), and after the nanoparticles are evenly distributed in the hydroxyl silicone oil, then add the boric acid particles, put them in a beaker and stir them thoroughly, and the stirring time is 0.5h;
[0049] (2) Pour the above-mentioned suspension system into an aluminum pan, and then place the aluminum pan on a heating plate with a constant temperature of 300°C. The mixed liquid no longer flows;
[0050] (3) After the reaction...
Embodiment 3
[0053] Preparation of PBDMS (filled with nano titanium dioxide) molecular colloid:
[0054] (1) Weigh nano-titanium dioxide, boric acid and hydroxy silicone oil with a mass ratio of 0.5:0.5:9.5, of which hydroxy silicone oil (Zhonghao Chenguang Chemical Research Institute, brand GY-209-3, polymerization degree 3-5) The quality of boric acid and nano-titanium dioxide (Henan Baililian Chemical Co., Ltd., trade mark is BLR-688) is 15g respectively. Add the nano-titanium dioxide into the hydroxyl silicone oil, stir at a high speed (800rpm / min), and after the nanoparticles are evenly distributed in the hydroxyl silicone oil, then add boric acid particles, put them in a beaker and stir thoroughly, and the stirring time is 0.5h;
[0055] (2) Pour the above-mentioned suspension system into an aluminum pan, and then place the aluminum pan on a heating plate with a constant temperature of 350°C. The mixed liquid in no longer flows;
[0056] (3) After the reaction was completed, the ma...
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