Preparation method of tobacco endogenous perfume and application thereof

An endogenous and flavoring technology, which is applied in the fields of tobacco, application, and preparation of tobacco, can solve the problems of cumbersome extraction methods, unclear extracts, and poor application effects, etc. The method is simple and practical, low in cost, and saves time. Effect

Active Publication Date: 2013-03-06

CHINA TOBACCO GUANGDONG IND

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AI-Extracted Technical Summary

Problems solved by technology

The extraction method is cumbersome and time-consuming, the extract i...

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Abstract

The invention discloses a preparation method of a tobacco endogenous perfume and application thereof. The tobacco endogenous perfume is prepared by carrying out column separation through adopting macroporous resin after carrying out ultrahigh-pressure extraction on crushed aromatic tobacco; and the prepared tobacco perfume has a clear appearance and is more suitable for the cigarette production. According to the invention, the method is simple and practical, is convenient to operate and is lower in cost; the resin can be repeatedly used; time is greatly saved; extracted effective aroma components have high value; and when the tobacco endogenous perfume is applied to cigarettes, the native aroma of the tobacco is increased, smoke is coordinated, the smoke is delicate and soft and the sweet feeling is increased.

Application Domain

Tobacco preparationTobacco treatment +1

Technology Topic

EngineeringSmoke +3

Image

Examples

Experimental program(7)
Effect test(1)

Example Embodiment

[0028] Example 1

[0029] (1) Take 300g of Baoshan Oriental Tobacco (Aromatic Oriental Tobacco Variety "Basma" ("Komatini" or "Kasaxi" Series, Central Grade One), which is grown in Baoshan, Yunnan, and crushed (about 50%) ~200 mesh) put into the ultra-high pressure extraction tank (UHP900ⅹ2 ultra-high pressure device is used in this example), add 10 times the volume ratio of 95% ethanol aqueous solution, soak the powder of Baoshan aromatic tobacco at room temperature for 30 minutes, pressurize to 100MPa, protect After pressing for 1 min, immediately release the pressure, repeat 3 times, filter the extract, and concentrate the filtrate to 450g.

[0030] (2) 500g of AB-8 macroporous resin, pre-load the column according to the instructions, (see http://www.tech-sep.com/a/techprofile/2011/1011/189.html), follow the steps ( 1) Load the 450g sample obtained with the flow rate controlled at 5mL/min, and then eluted with an ethanol aqueous solution with a volume ratio of 30%. The flow rate was controlled at 3mL/min, and the eluate was almost colorless. Collect the ethanol eluate. Concentrated to 30g, the endogenous flavor of Baoshan Oriental Tobacco is obtained.

Example Embodiment

[0031] Example 2

[0032] (1) Take 300g of Baoshan Oriental Tobacco (Central Grade 1) tobacco leaves, pulverize (about 50-200 mesh) into the ultra-high pressure extraction tank (same as Example 1), add 10 times the volume ratio of 95% ethanol aqueous solution , Soak Baoshan aromatic tobacco powder at room temperature for 30 minutes, pressurize to 100MPa, and release the pressure immediately after holding the pressure for 1 minute, repeat 3 times, filter the extract, and concentrate the filtrate to 450g.

[0033] (2) 500g of D101 macroporous resin, pre-load the column according to the instructions (http://www.sep-bj.com/news/html/?456.html), load the 450g sample obtained in step (1), The flow rate is controlled at 5mL/min, and then eluted with an ethanol aqueous solution with a volume ratio of 30%. The flow rate is controlled at 3mL/min, and the effluent is basically colorless. Collect the ethanol eluate and concentrate it to 30g. Endogenous flavors of tobacco.

Example Embodiment

[0034] Example 3

[0035] (1) Take 300g of Baoshan Oriental Tobacco (top second level) tobacco leaves, pulverize (about 50-200 mesh) into the ultra-high pressure extraction tank (UHP900ⅹ2 ultra-high pressure device), add 8 times the amount of water, soak at room temperature for 60 minutes, press to 600MPa, immediately relieve the pressure after 10 minutes of pressure retention, repeat 3 times, filter the extract, and concentrate the filtrate to 450g.

[0036] (2) 500g of ADS-17 macroporous resin, pre-load the column according to the instructions, load the 450g sample obtained in step (1), control the flow rate at 5mL/min, and then elute with a 40% volume ratio ethanol aqueous solution , The flow rate is controlled at 3mL/min, the effluent is basically colorless after washing, the ethanol eluate is collected and concentrated to 30g to obtain the endogenous flavor of Baoshan Oriental Tobacco.

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Description & Claims & Application Information

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Owner:FROG PRINCE (FUJIAN) BABY & CHILD CARE PROD CO LTD

Classification and recommendation of technical efficacy words

Simple method
Easy to operate

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Low cost Shorten the time Increase value Macroporous resin Food science Essential-oils/perfumes

Preparation method of tobacco endogenous perfume and application thereof

AI-Extracted Technical Summary

Problems solved by technology

Abstract

Image

Examples

Example Embodiment

Example Embodiment

Example Embodiment

PUM

Description & Claims & Application Information

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