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Method for synthesizing one-dimensional red long afterglow material

A long afterglow material and long afterglow luminescence technology, applied in the direction of luminescent materials, chemical instruments and methods, etc.

Inactive Publication Date: 2013-06-12
TAIYUAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
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Problems solved by technology

However, the amount of CS2 generated by this method is very small, resulting in a very small amount of yttrium hydroxide that can be vulcanized, and the prepared Y2O2 sub>S: Eu3+, Mg2+, Ti4+ Red long afterglow luminescent material only partially luminescent

Method used

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  • Method for synthesizing one-dimensional red long afterglow material
  • Method for synthesizing one-dimensional red long afterglow material
  • Method for synthesizing one-dimensional red long afterglow material

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Embodiment approach 1

[0045] Implementation mode 2:

Embodiment approach 2

[0047] Implementation mode 3:

Embodiment approach 3

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Abstract

The invention discloses a method for synthesizing a one-dimensional red long afterglow material, and belongs to the technical field of preparation of a phosphor material. The method is characterized by comprising the steps of carrying out hydrothermal reaction on Y3<+>, Eu<3+>, Mg<2+>, and Ti<4+> at the same time to generate a Y(OH)3 precursor doped with Eu<3+>, Mg<2+>, and Ti<4+>, vulcanizing the precursor by mixture of carbon powder and sublimed sulfur to generate a one-dimensional Y2O2S:Eu<3+>, Mg<2+>, and Ti<4+> red long afterglow luminescent material. The red long afterglow luminescent material prepared by the method disclosed by the invention is low in crystallization temperature of the substrate; ions which need to be doped are doped into the substrate at the hydrothermal stage of fabricating the precursor; the good nano tubular structure of a sample can be kept in later vulcanizing and sintering processes; and the physical and chemical properties are stable.

Description

technical field [0001] The invention discloses a method for synthesizing a one-dimensional red long-lasting luminescent material, which belongs to the technical field of phosphorescent material preparation, and specifically relates to a method for combining Y 3+ 、Eu 3+ , Mg 2+ and Ti 4+ At the same time, the hydrothermal reaction produces Eu 3+ , Mg 2+ and Ti 4+ Doped Y(OH) 3 precursor, followed by sulfuration of Y(OH) with a mixture of carbon powder and sublimated sulfur 3 Prebody generation 1D Y 2 o 2 S: Eu 3+ , Mg 2+ , Ti 4+ Red long-lasting glow material approach. Background technique [0002] Rare-earth long-lasting luminescent materials can store energy under sunlight, and then slowly release energy in a dark background to emit light. This feature is widely used in low-light lighting, emergency instructions, architectural decoration and other fields. In recent years, Later, it gradually expanded to high-tech fields such as optical information storage...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K11/84
Inventor 崔彩娥王磊黄平姜国伟武银兰郝虎在
Owner TAIYUAN UNIV OF TECH
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