Ho-doped ScVO4 luminous material and crystal growth method for same using melt method
A technology for crystal growth and luminescent materials, applied in crystal growth, luminescent materials, polycrystalline material growth, etc., can solve problems such as low efficiency, and achieve the effects of saving production costs, easy operation, and low equipment requirements
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[0017] Preparation of HozSc with Ho doping concentration of 0.5 at% 1-z VO 4 Single crystal:
[0018] (1) Using Ho 2 o 3 、Sc 2 o 3 , V 2 o 5 As a raw material, carry out batching according to the following compound formula:
[0019]
[0020] The composition of each component of this raw material is as follows:
[0021] Ho 2 o 3 0.35%
[0022] sc 2 o 3 65.9553 %
[0023] V 2 o 5 33.6947%
[0024] And these raw materials are fully mixed evenly to obtain the ingredient mixture.
[0025] (2) Using Ho 2 o 3 、Sc 2 o 3 , V 2 o 5 As the raw material, the ingredients are mixed according to the following compound formula. After they are fully mixed, they are pressed, pre-fired at 60°C for 51 minutes, pressed again, and then sintered after cooling: the re-sintering temperature is 980°C, and the sintering time is After 48 hours, the polycrystalline raw materials required for growing crystals were obtained:
[0026] (3) Put the initia...
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