Separation method of chloropentafluoroethane and pentafluoroethane
A technology of monochloropentafluoroethane and pentafluoroethane, which is applied in the field of separation of monochloropentafluoroethane and pentafluoroethane, can solve uneconomical problems, reduce energy consumption, optimize process flow, and stabilize The effect of production
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Embodiment 1
[0037] This embodiment provides a method for separating a mixture of chloropentafluoroethane and pentafluoroethane according to the above-mentioned process flow, and the raw materials and process conditions are as follows:
[0038] (1) In the mixture of chloropentafluoroethane and pentafluoroethane to be separated: the content of chloropentafluoroethane is 1wt%, the content of pentafluoroethane is 98.5wt%, tetrafluoroethane and its The homologue content is 3 / h;
[0039] (2) Extractant: petroleum hydrocarbon;
[0040] (3) Parameter setting of the primary extractive distillation column: the feed rate of the mixture of chloropentafluoroethane and pentafluoroethane to be separated is 2.4~2.6m 3 / h, the throughput of extractant is 8~11 m 3 / h, pressure 0.8~1.2MPa, return flow 4~7 m 3 / h;
[0041] Parameter setting of the secondary extractive distillation column: the feed rate of the mixture containing chloropentafluoroethane and pentafluoroethane is 0...
Embodiment 2
[0047] This embodiment provides a method for separating a mixture of chloropentafluoroethane and pentafluoroethane according to the above-mentioned process flow, and the raw materials and process conditions are as follows:
[0048] (1) In the mixture of chloropentafluoroethane and pentafluoroethane to be separated, the content of chloropentafluoroethane is 1.5 wt%, the content of pentafluoroethane is 98 wt%, tetrafluoroethane and its Congener content 3 / h;
[0049] (2) Extractant: petroleum ether (C 3 -C 6 ethers);
[0050] (3) Parameter setting of the primary extractive distillation column: the feed rate of the mixture of chloropentafluoroethane and pentafluoroethane to be separated is 2.4~2.6m 3 / h, the throughput of the extractant is 7~9m 3 / h, pressure 1.2~1.4 MPa, return flow 5~8 m 3 / h ;
[0051] Parameter setting of the secondary extractive distillation column: the feed rate of the mixture 7 containing chloropentafluoroethane and p...
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