A test paper for quickly judging rice freshness and its application
A technology of freshness and test paper, which is applied in the direction of analyzing materials through chemical reactions and observing the influence of chemical indicators on materials, etc. It can solve problems such as water absorption reduction, darkening of color, and viscosity drop. Achieve the effects of simplifying the method of adsorbing rice volatiles, avoiding interference with the production of volatiles, and simple preparation process
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Embodiment 1
[0033] Step 1. Immerse blank filter paper in 2,4-dinitrophenylhydrazine hydrochloric acid-methanol solution (2,4-dinitrophenylhydrazine concentration is 5 mg / L, hydrochloric acid volume fraction is 1.5%) at room temperature for 2 minutes, Then take it out, let it dry for 30 seconds, and cut out two test papers with a size of 2cm×5cm to obtain test paper A and test paper B;
[0034] Step 2. Weigh 10g of rice sample (place of origin: Guangdong; conventional storage for 2 years), put the rice sample and test paper A into 150mL conical flask A, and put test paper B into 150mL conical flask B separately;
[0035] Step 3: Seal the mouths of the two Erlenmeyer flasks with tin foil, and then heat the two Erlenmeyer flasks in a 50°C water bath for 10 minutes;
[0036] Step 4, take out test paper A and test paper B, and read the test results. Compared with test paper B: test paper A is obviously yellow, and the rice sample is old rice.
[0037] Test result verification:
[0038] (1) P...
Embodiment 2
[0042] Step 1. Immerse blank filter paper in 2,4-dinitrophenylhydrazine hydrochloric acid-methanol solution (2,4-dinitrophenylhydrazine concentration is 25mg / L, hydrochloric acid volume fraction is 1.5%) at room temperature for 1.5min , then take it out, let it dry for 25 seconds, cut two test papers with a size of 3cm×6cm, and obtain test paper A and test paper B;
[0043] Step 2: Weigh 15g of rice sample (origin: Guangdong; regular storage for half a year), put the rice sample and test paper A into 150mL conical flask A, and put test paper B into 150mL conical flask B separately;
[0044] Step 3: Seal the mouths of the two Erlenmeyer flasks with tin foil, and then heat the two Erlenmeyer flasks in a 60°C water bath for 20 minutes;
[0045] Step 4, take out test paper A and test paper B, and read the test results. Compared with test paper B: test paper A obviously does not show color, and the rice sample is new rice.
[0046] Test result verification:
[0047] (1) Prepare t...
Embodiment 3
[0051] Step 1: Immerse the blank filter paper in the hydrochloric acid-methanol solution of 2,4-dinitrophenylhydrazine (2,4-dinitrophenylhydrazine concentration is 50mg / L, the volume fraction of hydrochloric acid is 1.5%) at room temperature for 1min, Then take it out, let it dry for 35 seconds, and cut out 4 test papers with a size of 4cm×8cm to obtain test paper A, test paper B, test paper C and test paper D;
[0052] Step 2: Weigh 20g of newly harvested rice (origin: Guangdong) (rice sample A), 20g of rice stored for 1 year (rice sample B, produced in Hunan), and 20g of rice stored for 2 years (rice sample C, produced in Jiangxi ), then put rice sample A and test paper A into 150mL Erlenmeyer flask A, rice sample B and test paper B into 150mL Erlenmeyer flask B, rice sample C and test paper C into 150mL Erlenmeyer flask C, and test paper D separately into a 150mL Erlenmeyer flask D;
[0053] Step 3: Seal the mouths of the four Erlenmeyer flasks with tin foil, and then heat...
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