Production method of sustained release aramid nano-microcapsule cellulosic fiber
A cellulose fiber and nano-sustained-release technology, applied in the fiber field, can solve the problems of short duration of fragrance and restrictions on popularization and application, and achieve the effect of long duration of fragrance
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Embodiment 1
[0008] Embodiment 1: Weigh 25 grams of nano-sustained-release aromatic microcapsule mother liquor (the mass percentage concentration is 20%) and add it to 50 grams of desalinated water. ℃ -55 ℃ to make nano-sustained-release aromatic microcapsule emulsion with good stability, and then add MT-84 dispersant, which accounts for 0.01% of the mass of nano-sustained-release aromatic microcapsules, stir for 5 hours, and mix evenly. The mass percentage concentration is: 5% nano-sustained-release aromatic microcapsule suspension is then added into the stirring tank, the pre-spinning injection device is turned on, and the nano-sustained-release aromatic microcapsule suspension and the cellulose sulfonate solution are uniformly mixed through the pre-spinning injection device. To 1120 grams of cellulose sulfonate solution (mass percentage: methyl fiber 8.1%, alkali 6%), 10 grams of nano-sustained-release aromatic microcapsule suspension with a mass percentage concentration of 5% was added....
Embodiment 2
[0009] Example 2: Weigh 50 grams of nano-sustained-release aromatic microcapsule mother liquor (with a mass percentage concentration of 20%) and add it to 50 grams of desalinated water. ℃ -55 ℃ to make nano-sustained-release aromatic microcapsule emulsion with good stability, then add MT-84 dispersant accounting for 0.03% of the mass of nano-sustained-release aromatic microcapsules, stir for 5 hours, and mix evenly, the mass percentage concentration is: 10% nano-sustained-release aromatic microcapsule suspension is then added into the stirring tank, the pre-spinning injection device is turned on, and the nano-sustained-release aromatic microcapsule suspension and the cellulose sulfonate solution are uniformly mixed through the pre-spinning injection device. To 1120 grams of cellulose sulfonate solution (methyl fiber 8.1%, alkali 6%), 50 grams of nano-sustained-release aromatic microcapsule suspension with a concentration of 10% by mass was added. Through the spinning bath: 140...
Embodiment 3
[0010] Embodiment 3: Weigh 75 grams of nano-sustained-release aromatic microcapsule mother liquor (the mass percentage concentration is 20%) and add it to 25 grams of desalinated water. ℃ -55 ℃ to make nano-sustained-release aromatic microcapsule emulsion with good stability, and then add MT-84 dispersant, which accounts for 0.05% of the mass of nano-sustained-release aromatic microcapsules, stir for 5 hours, and mix evenly. The mass percentage concentration is: 15% nano-sustained-release aromatic microcapsule suspension is then added into the stirring tank, the pre-spinning injection device is turned on, and the nano-sustained-release aromatic microcapsule suspension and the cellulose sulfonate solution are uniformly mixed through the pre-spinning injection device. To 1500 grams of cellulose sulfonate solution (weight percent: methyl fiber 8.1%, alkali 6%), add 100 grams of nano-sustained-release aromatic microcapsule suspension with a concentration of 15% by weight. Through ...
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