A preparation method of strain sensor based on carbon nanotube three-dimensional network film

A strain sensor and carbon nanotube technology, applied in the field of material science, can solve the problems affecting the construction of sensing network, the increase of resin matrix viscosity, and the mechanical properties of composite materials, etc., and achieve excellent strain sensing accuracy and linear repeatability Effect

Inactive Publication Date: 2016-05-25
SHENYANG AEROSPACE UNIVERSITY
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the carbon nanotubes are directly dispersed in the polymer matrix, and the strain is monitored through the resistance change of the composite material, the strain and resistance of the carbon nanotube composite material can show a good linear relationship, but the intermolecular force of the carbon nanotubes is relatively large , when directly dispersed in the polymer matrix, its huge specific surface area will lead to an increase in the viscosity of the resin matrix, making it difficult to form the composite material, thereby affecting the mechanical properties of the composite material. At the same time, due to the low content of carbon nanotubes, it is difficult to disperse And other issues will also affect the construction of carbon nanotube sensing network and sensing accuracy

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A preparation method of strain sensor based on carbon nanotube three-dimensional network film
  • A preparation method of strain sensor based on carbon nanotube three-dimensional network film
  • A preparation method of strain sensor based on carbon nanotube three-dimensional network film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] refer to figure 1 , figure 2 , a method for preparing a strain sensor based on a carbon nanotube three-dimensional network film, which is achieved through the following steps:

[0021] a. A mixture of carbon nanotubes and a surface dispersant is used to prepare a monodisperse aqueous solution of carbon nanotubes by mechanical fusion, wherein the carbon nanotubes are multi-walled carbon nanotubes, the surfactant is TX-100, and the concentration of the aqueous solution of the carbon nanotubes Controlled at 0.1wt%, surfactant: carbon nanotube mass ratio = 5:1, mechanical fusion method mainly includes body grinding, magnetic stirring, ultrasonic dispersion, high-speed centrifugation.

[0022] b. Pour the monodisperse aqueous solution of carbon nanotubes into the upper container of the vacuum suction filter device and filter it on the filter membrane to form a membrane. The filter membrane is selected from 0.22PTFE membrane, and the vacuum degree is controlled to be 60kpa....

Embodiment 2

[0030] refer to figure 1 , figure 2 , a method for preparing a strain sensor based on a carbon nanotube three-dimensional network film, which is achieved through the following steps:

[0031] a. A mixture of carbon nanotubes and a surface dispersant is used to prepare a monodisperse aqueous solution of carbon nanotubes by mechanical fusion, wherein the carbon nanotubes are selected from multi-walled carbon nanotubes, single-walled carbon nanotubes, and functionalized carbon nanotubes. TX-100, SDS, SDBS are selected as the agent, the concentration of the aqueous solution of carbon nanotubes is controlled at 0.01wt%, the surfactant: carbon nanotubes (mass ratio) = 20:1, and the mechanical fusion method mainly includes mortar grinding, magnetic stirring, Ultrasonic dispersion, high-speed centrifugation.

[0032] b. Pour the monodisperse aqueous solution of carbon nanotubes into the upper container of the vacuum suction filter device and filter on the filter membrane to form a ...

Embodiment 3

[0037] refer to figure 1 , figure 2 , a method for preparing a strain sensor based on a carbon nanotube three-dimensional network film, which is achieved through the following steps:

[0038] a. A mixture of carbon nanotubes and a surface dispersant is used to prepare a monodisperse aqueous solution of carbon nanotubes by mechanical fusion, wherein the carbon nanotubes are selected from multi-walled carbon nanotubes, single-walled carbon nanotubes, and functionalized carbon nanotubes. TX-100, SDS, SDBS are selected as the agent, the concentration of the aqueous solution of carbon nanotubes is controlled at 2.5wt%, the surfactant: carbon nanotubes (mass ratio) = 5:1, and the mechanical fusion method mainly includes mortar grinding, magnetic stirring, Ultrasonic dispersion, high-speed centrifugation.

[0039] b. Pour the monodisperse aqueous solution of carbon nanotubes into the upper container of the vacuum suction filtration device and filter on the filter membrane to form ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
pore sizeaaaaaaaaaa
electrical resistivityaaaaaaaaaa
pore sizeaaaaaaaaaa
Login to view more

Abstract

The invention discloses a temperature sensor preparation method based on a carbon nano tube three-dimensional network film. The strain sensor preparation method mainly solves the problems that the carbon nano tube sensing technology based on the external of the polymer can affect the composite material molding and composite material mechanical property. The strain sensor preparation method comprises the following realization steps of: a) preparing monodisperse aqueous solution by mechanically mixing the mixture of the carbon nano tube and surface dispersant; b) pouring the monodisperse aqueous solution of the carbon nano tube into a container of a vacuum suction filtration device, and carrying out suction filtration to form a film on a filtering film; c) compacting a carbon nano film and the filtering film, putting a carbon nano film and the filtering film into a drying oven for solidifying, and stripping the filtering film to obtain a three-dimensional film after solidification is finished; and d) cutting a rectangular structure from the film, fixing a lead onto the surface of the carbon nano tube film by, embedding the sensor into the specific position in the external of the composite material, and forming according to the composite material solidification technology. The the carbon nano tube three-dimensional film strain sensor has good interface combination properties, high strain sensing accuracy and linear repeatability, can be molded with the composite materials, and is applicable to monitor strain filed of the external structure.

Description

technical field [0001] The invention relates to a method for preparing a sensor, in particular to a method for preparing a strain sensor based on a carbon nanotube three-dimensional thin film, and belongs to the technical field of material science. Background technique [0002] Carbon nanotubes are excellent sensor materials due to their excellent thermodynamic properties, piezoresistive properties and electrical properties. When the carbon nanotubes are directly dispersed in the polymer matrix, and the strain is monitored through the resistance change of the composite material, the strain and resistance of the carbon nanotube composite material can show a good linear relationship, but the intermolecular force of the carbon nanotubes is relatively large , when directly dispersed in the polymer matrix, its huge specific surface area will lead to an increase in the viscosity of the resin matrix, making it difficult to form the composite material, thereby affecting the mechanic...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): G01B7/16
Inventor 卢少微贲强张海军高禹聂鹏吕伟
Owner SHENYANG AEROSPACE UNIVERSITY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products