Preparation method of optical fiber covering quartz capillary perform and continuous melting furnace equipment

A quartz capillary and preform technology, applied in glass manufacturing equipment, manufacturing tools, glass molding, etc., can solve the problems of products failing to meet the international quality standards of similar products, air bubbles, gas lines, etc.

Active Publication Date: 2014-06-25
LIANYUNGANG HONGYANG QUARTZ PROD
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  • Abstract
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  • Application Information

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Problems solved by technology

In the existing technology, most of my country's optical fiber preforms are imported, which are restricted and restricted by foreign companies, and the products produced by domestic manufacturers cannot meet the quality standards of similar international products.
However, the domestically produced quartz outer cladding tube will produce defects such as air bubbles and air lines during the drawing process, which seriously affects the yield of the preform in the optical fiber drawing process.

Method used

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  • Preparation method of optical fiber covering quartz capillary perform and continuous melting furnace equipment

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Experimental program
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Embodiment Construction

[0019] A method for outsourcing an optical fiber with a quartz capillary preform,

[0020] Preparation of High Purity Quartz Sand

[0021] The rough stone is crushed to a quartz stone with a block diameter of less than 30mm, then acid-leaved for 48 hours, taken out and dried, put into a furnace, quenched with deionized water, and then dried at 250°C;

[0022] Put the dried quartz stone into the roller machine for crushing, sort out the quartz sand with a mesh number between 30 and 100 mesh and put it into a mixed acid for 24 to 36 hours. The mixed acid is hydrochloric acid, hydrofluoric acid, etc. The mixed acid of acid and oxalic acid, wherein the mass ratio of hydrochloric acid: hydrofluoric acid: oxalic acid is 1:1~10:1~3, the mass percentage concentration of mixed acid is 10~20%; the amount of mixed acid is the mass of quartz sand 20~25%;

[0023] Wash the quartz sand soaked in mixed acid with deionized water, then dry it, go through multi-stage high gradient magnetic se...

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Abstract

The invention discloses a method of an optical fiber covering quartz capillary perform. The method comprises the following steps: firmly, preparing high-purity quartz sand with SiO2 content not less than 99.9999%; then, melting, drawing and forming through a continuous melting furnace, wherein a special former is formed by combining a middle cylindrical section and a lower frustum-shaped section; the drawn and formed optical fiber covering quartz capillary perform is 0.1-0.2mm in inner hole diameter, 0.05mm in outside diameter tolerance and 0.02mm in thickness deviation, and the perform, after being treated by dehydroxylation, is not more than 1ppm in hydroxyl value. By rice natural crystal raw materials in China, the preparation method realizes domestication of optical fiber covering pipes; the excellent high-quality and high-purity optical fiber covering quartz capillary perform produced by the method completely achieves a quality standard of international similar products.

Description

technical field [0001] The invention relates to a preparation technology of quartz, in particular to a preparation method of a quartz capillary prefabricated rod covered with an optical fiber and a continuous melting furnace equipment. Background technique [0002] Optical fiber is a light transmission tool that relies on the principle of total reflection of light in the medium. With the vigorous development of my country's communication industry, the demand for optical fiber in my country is second only to the United States, and it will become the largest market in the optical fiber industry in the world in the future. Optical fiber is made of pre-prepared preform rods drawn by various methods and then coated with various polymer materials. Manufacturing preform rods is a key technology in optical fiber production. In the existing technology, most of my country's optical fiber preforms are imported, which are restricted and restricted by foreign companies, and the products ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B37/012C03B20/00
Inventor 徐传龙王丽熙刘云飞
Owner LIANYUNGANG HONGYANG QUARTZ PROD
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