Method for preparing drilling fluid lubricant for reducing extreme pressure friction and mud cake adhesive friction
A mud cake lubrication improvement and drilling fluid technology, which is applied in the fields of oil and natural gas and geological exploration, can solve problems such as no lubricant products, and achieve the effects of good mud cake adhesion and lubrication ability, reducing dosage and ensuring underground safety.
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Embodiment 1
[0049] Put nonylphenol polyoxyethylene ether with a degree of polymerization of 4 (hereinafter referred to as OP-4) and polyphosphoric acid in a molar ratio of 4:1 in a reaction vessel, stir at 70°C for 30 minutes, then raise the temperature to 100°C and stir for 30 minutes. Then cooled to room temperature to prepare the extreme pressure additive with surface activity. In the extreme pressure additive, the molar ratio of each component is: OP-4-PO 3 h 2 :OP-4:H 3 PO 4 =3:1:1, OP-4-PO 3 h 2 for C 9 h 19 C 6 h 4 O(C 2 h 4 O) 4 PO 3 h 2 .
Embodiment 2
[0051] Put nonylphenol polyoxyethylene ether with a degree of polymerization of 7 (hereinafter referred to as OP-7) and polyphosphoric acid in a molar ratio of 4:1 in a reaction vessel, stir at 50°C for 60 minutes, then raise the temperature to 150°C, and stir for 20 minutes , and then cooled to room temperature to obtain a surface active extreme pressure additive. The molar ratio of each component in the extreme pressure additive is: OP-7-PO 3 h 2 :OP-7:H 3 PO 4 =3:1:1,OP-7-PO 3 h 2 for C 9 h 19 C 6 h 4 O(C 2 h 4 O) 7 PO 3 h 2 .
Embodiment 3
[0053] Put nonylphenol polyoxyethylene ether (OP-10) with a degree of polymerization of 10 and polyphosphoric acid in a molar ratio of 4:1 in a reaction vessel, stir at 50°C for 1 hour, then heat up to 90°C and stir for 2 hours, then cool to room temperature to obtain a surface active extreme pressure additive. The molar ratio of each component in the extreme pressure additive is: OP-10-PO 3 h 2 :OP-10:H 3 PO 4 =3:1:1,OP-10-PO 3 h 2 for C 9 h 19 C 6 h 4 O(C 2 h 4 O) 10 PO 3 h 2 .
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