Modified phenolic resin material for 3D printing and preparation method thereof
A phenolic resin, 3D printing technology, applied in the field of 3D printing materials and their preparation, can solve the problems of single performance improvement, affecting the modification effect, unable to meet the 3D printing technology, etc., to achieve lower operating temperature, low production cost, and chain extension and the effect of simple and controllable cross-linking degree
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[0042] Example 1
[0043] 1) Add 70 parts of novolak resin (molecular weight 600) and 7 parts of polybutyl methacrylate oligomer with molecular weight of 350 to the blender, raise the temperature to 80°C, add 0.2 parts of chain extender and 0.4 parts of Blocking agent, react for half an hour, then add 0.2 parts of cross-linking agent and 7 parts of reinforcing agent, fully mix for 1 hour at a speed of 600r / min, and then discharge;
[0044] 2) Mix the mixture obtained in step 1) with 12 parts of toughening agent, 3 parts of lubricant and 0.2 parts of stabilizer with a twin-screw extruder for mixing, extruding and granulating. The time of the material in the extruder does not exceed 3 minute. The screw diameter of the twin-screw extruder is 71mm, the extruder temperature is set to 150-170℃, and the die temperature is 170-180℃:
[0045] 3) Dry the particles produced in step 2) at a temperature of 50°C for 2-3 hours and then extrude them with a twin-screw extruder into filaments with d...
Example Embodiment
[0046] Example 2
[0047] 1) Add 75 parts of novolac resin (molecular weight 600) and 7 parts of polybutyl methacrylate oligomer with molecular weight of 350 to the mixer, increase the temperature to 80°C, add 0.2 parts of chain extender and 0.6 parts of sealing agent in turn Ending agent, react for half an hour, then add 0.2 parts of cross-linking agent and 7 parts of reinforcing agent, fully mix for 1 hour under the condition of rotation speed of 600r / min, and then discharge;
[0048] 2) Mix the mixture obtained in step 1) with 12 parts of toughening agent, 3 parts of lubricant and 0.2 parts of stabilizer with a twin-screw extruder for mixing, extruding and granulating. The time of the material in the extruder does not exceed 3 minute. The screw diameter of the twin-screw extruder is 71mm, the extruder temperature is set to 150-170℃, and the die temperature is 170-180℃:
[0049] 3) Dry the particles produced in step 2) at a temperature of 50°C for 2-3 hours and then extrude them ...
Example Embodiment
[0050] Example 3
[0051] 1) Add 80 parts of novolac resin (molecular weight 600) and 7 parts of polybutyl methacrylate oligomer with molecular weight of 350 to the blender, increase the temperature to 80°C, and add 0.2 parts of chain extender and 0.6 parts of sealing agent in sequence. Ending agent, react for half an hour, then add 0.2 parts of cross-linking agent and 7 parts of reinforcing agent, fully mix for 1 hour under the condition of rotation speed of 600r / min, and then discharge;
[0052] 2) Mix the mixture obtained in step 1) with 12 parts of toughening agent, 3 parts of lubricant and 0.2 parts of stabilizer with a twin-screw extruder for mixing, extruding and granulating. The time of the material in the extruder does not exceed 3 minute. The screw diameter of the twin-screw extruder is 71mm, the extruder temperature is set to 150-170℃, and the die temperature is 170-180℃:
[0053] 3) Dry the particles produced in step 2) at a temperature of 50°C for 2-3 hours and then ex...
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