Observation method of B-type inclusion behaviors in aluminum killed steel

A technology for aluminum-killed steel and inclusions, applied in the field of metallurgy, can solve the problems of poor control effect of B-type inclusions, difficult to effectively observe the formation of B-type inclusions, etc.

Inactive Publication Date: 2014-10-15
SHOUGANG CORPORATION
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Problems solved by technology

At present, due to the unclear formation mechanism of B-type inclusions, it is difficult to effectively observe the formation of B-type inclusions, so the control effect on B-type inclusions in aluminum-killed steel is poor

Method used

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  • Observation method of B-type inclusion behaviors in aluminum killed steel
  • Observation method of B-type inclusion behaviors in aluminum killed steel

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Embodiment Construction

[0016] see figure 1 , The high-temperature laser confocal microscope includes: imaging system, vacuum system, inert gas purification system, metallographic heating furnace and temperature control system, among which the temperature control system includes R-type thermocouples. The embodiment of the present invention uses a high-temperature laser confocal microscope to observe the behavior of B-type inclusions in aluminum-killed steel.

[0017] see figure 2 , a method for observing the behavior of B-type inclusions in aluminum-killed steel provided in an embodiment of the present invention, specifically includes the following steps:

[0018] Step 10: Prepare an aluminum-killed steel sample by wire cutting. The aluminum-killed steel sample is in the shape of a cylinder with a diameter of 6-7.5 mm and a height of 1-3 mm.

[0019] Step 20: Roughly grind and finely grind the surface of the aluminum-killed steel sample, and use a diamond polishing agent to polish the surface of t...

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Abstract

The invention relates to the technical field of metallurgy, particularly to an observation method of B-type inclusion behaviors in aluminum killed steel. The method comprises the steps as follows: preparing an aluminum killed steel sample, and performing coarse grinding, fine grinding, polishing and cleaning on the surface of the sample; placing the sample in a metallographic heating furnace of a high-temperature laser confocal microscopic; performing vacuum pumping treatment on the metallographic heating furnace and then feeding an inert gas continuously; performing radiation heating and real-time temperature measurement on the sample; heating the sample to 1550-1600 DEG C, keeping the sample at the constant temperature for 120-600 s, and then continuously cooling the sample at the speed of 0.2-1 DEG C / s; irradiating the surface of the aluminum killed steel sample by a laser beam, and performing high-speed scanning and observation on the surface of molten steel in the cooling process by the high-temperature laser confocal microscopic. With the adoption of the observation method of the B-type inclusion behaviors in the aluminum killed steel, the forming process of B-type inclusions in the aluminum killed steel can be observed clearly and conveniently, and a basis is provided for the research and the control on the B-type inclusions in the aluminum killed steel.

Description

technical field [0001] The invention relates to the technical field of metallurgy, in particular to an observation method for the behavior of B-type inclusions in aluminum-killed steel. Background technique [0002] Exceeding the standard of type B inclusions is a common problem faced by current medium and heavy plate enterprises. At present, the non-compliance rate of inclusions in the pipeline steel of enterprises with the best control level is as high as about 2%, among which CaO-Al is mainly 2 o 3 Department of B-type inclusions. The existence of B-type inclusions in aluminum-killed steel is inseparable from the steelmaking and refining processes commonly used at present. In order to control the cleanliness of molten steel, aluminum with strong deoxidation ability is mainly used for deoxidation in steelmaking, and the aluminum oxide inclusions formed are very easy. Sticking to the side wall of the nozzle, causing blockage. In order to avoid alumina sticking and plugg...

Claims

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Application Information

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IPC IPC(8): G01N21/88
Inventor 邵肖静李海波季晨曦其其格崔阳朱国森高攀李飞包春林陈斌唐德池刘柏松徐颖
Owner SHOUGANG CORPORATION
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