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A kind of preparation method of ti-nb-fe-o high damping alloy

A technology of ti-nb-fe-o, high damping alloy, applied in the field of high damping alloy and its preparation, can solve the problems of uncontrollable TiO2 loss, relaxation reversibility or relaxation strength decrease, and alloy damping performance deterioration, etc. Achieve precise and controllable components, enhance mechanical properties, and improve service life.

Active Publication Date: 2016-01-27
TIANJIN YINLONG HIGH TECH NEW MATERIAL RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition to the mechanical properties that need to be improved, it is also found in continuous and in-depth research that these high-damping alloys show a common problem in terms of service stability and damping delay: that is, low-dimensional defects in the system (mainly Interstitial atoms and vacancies) are diffusely redistributed under the induction of continuous vibration loads, and gradually enrich in high-dimensional defect regions (such as dislocations, magnetic domain boundaries, (twin) grain boundaries), resulting in pinning, resulting in The relaxation reversibility or relaxation strength of high-dimensional defects gradually decreases or even loses to a certain extent under the action of vibration load, which eventually leads to serious deterioration of the damping performance of the alloy and shortens the service life.
However, this method cannot control the TiO 2 loss, so that the final alloy composition is difficult to control

Method used

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  • A kind of preparation method of ti-nb-fe-o high damping alloy
  • A kind of preparation method of ti-nb-fe-o high damping alloy

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Example 1: The mass percentage (wt.%) of the alloy composition in the Ti-Nb-Fe-O high damping alloy is: Ti: 74.1, Nb: 15.3, Fe: 10.5, O atom solid solution: 0.10.

Embodiment 2

[0029] Example 2: The mass percentage (wt.%) of the alloy composition in the Ti-Nb-Fe-O high damping alloy is: Ti: 70.42, Nb: 12.4, Fe: 17.1, O atom solid solution: 0.08.

Embodiment 3

[0030] Example 3: The mass percentage (wt.%) of the alloy composition in the Ti-Nb-Fe-O high damping alloy is: Ti: 64.74, Nb: 11.0, Fe: 24.2, O atom solid solution: 0.06.

[0031] The concrete preparation steps of above-mentioned embodiment are as follows:

[0032] 1. Matrix alloy melting

[0033] According to the ratio of Ti-Nb-Fe matrix alloy, the Ti-Nb master alloy is first melted in a high-vacuum arc melting furnace with a vacuum degree of 0.01Pa and argon protection, and then Fe is added to melt into a Ti-Nb-Fe matrix alloy.

[0034] 2. Vacuum heat treatment of base alloy

[0035] The obtained Ti-Nb-Fe matrix alloy is placed in a vacuum heat treatment furnace with a vacuum degree of 0.01Pa, the vacuum heat treatment temperature is 900°C, and the heat treatment time is 1 hour, so that the Ti-Nb-Fe matrix alloy is fully homogenized.

[0036] 3. Cold rolling deformation treatment of base alloy

[0037] The homogenized Ti-Nb-Fe matrix alloy is cold-rolled and deformed by a...

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Abstract

The invention relates to high-damping Ti-Nb-Fe-O alloy and a preparation method thereof. The preparation method comprises the following steps: adding atomic Fe into Ti-Nb alloy to prepare a Ti-Nb-Fe base body, performing surface oxygen solution treatment, diffusing oxygen through a controllable atmosphere to enable oxygen to enter Ti-Nb-Fe base body alloy to form a remarkable oxygen solution layer, and forming a surface oxidation region in a single beta-Ti-phase base body, a double-phase region in the middle and an oxygen-enrichment solid-solution beta-Ti region in a core part. The alloy comprises the following components by weight percent: 60%-75% of Ti, 10%-16% of Nb, 10%-25% of Fe and 0.05%-0.10% of O. The alloy has good damping characteristics. The preparation method of the alloy is low in cost, high in efficiency and simple in process, and the components are accurate and controllable. The alloy is suitably applied to damping structure parts with relatively high service environment temperature.

Description

technical field [0001] The invention relates to a high damping alloy and a preparation method thereof, more specifically, to a Ti-Nb-Fe-O high damping alloy and a preparation method thereof. Background technique [0002] With the rapid development of modern industry, all kinds of mechanical equipment require higher precision and longer service life, while vibration and noise will seriously affect the precision and service life of the equipment. Therefore, in recent years, damping alloys used for vibration and noise control have attracted the attention of industrialized countries in the world, and have developed rapidly. [0003] In the past 50 years of continuous research, according to the attenuation mode of vibration energy caused by different types of structural defects inside the material, three types of traditional high-damping alloys have been roughly formed, that is, dislocation-type high-damping alloys (such as Mg-Zr system high-damping alloys). Damping alloys, Al-Z...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C14/00C22F1/18
Inventor 谢志峰余黎明冀璞光
Owner TIANJIN YINLONG HIGH TECH NEW MATERIAL RES INST
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