Wood-vinegar alkaline insecticide composition and preparation method thereof
A technology of insecticide and composition, applied in the field of wood vinegar base insecticide composition and its preparation, can solve the problems of designing inhibitor insecticides, etc., and achieve the effect of low toxicity and improved insecticidal effect
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[0039] (1) Preparation of rectification oak wood vinegar:
[0040] a. Carry out dry distillation of fresh oak wood, collect steam gas, condense and separate, and collect liquid products;
[0041] b. After precipitating the liquid product collected in step a for 48 hours, add activated carbon for adsorption for 20 hours;
[0042] c. Rotary evaporation at 39.5°C, the evaporation pressure is -0.35kPa, and the remaining volume is 30% of the original volume;
[0043] d. Use a cellulose acetate organic filter membrane with a pore size of 0.1 μm to filter the rotary evaporated liquid twice to obtain clear and transparent yellow oak wood vinegar.
[0044] (2) Preparation of benzaldehyde amino L-cysteine Schiff base:
[0045] First add 5ml of distilled water to 20mmol (about 2.423g) of L-cysteine and stir to make it dissolve to the greatest extent, then add 90ml of absolute ethanol and stir. Add 2.0ml benzaldehyde (density 1.044-1.047, concentration 98.5%, molecular weight 106.1...
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