A method for flame-retardant finishing of fleece polyester fabrics for high-speed rail and train seats
A flame retardant finishing, motor vehicle technology, applied in fiber processing, textiles and papermaking, fiber types, etc., can solve the problems of large amount of smoke, molten droplets, corrosion, etc., to improve flame retardant performance, good flame retardant performance Effect
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Embodiment 1
[0029] (1) Preparation of flame retardant composite sol-gel. The silica sol was synthesized from sodium silicate, the alumina sol was synthesized from aluminum isopropoxide, and then a silica-alumina composite sol was obtained by mixing the two.
[0030] (i) Silica sol preparation
[0031] Add 0.03mol sodium silicate and 50mL water into the reactor, stir vigorously at room temperature for 10min, then add 10ml of 36% hydrochloric acid dropwise, and continue vigorously stirring for 5h to obtain a stable, uniform and transparent silica sol;
[0032] (ii) Preparation of alumina sol
[0033] Add 0.02mol aluminum isopropoxide and 100mL water into the reactor, stir vigorously at 80°C, evaporate for 20-30min to remove most of the alcohol, slowly add 2ml of 95% nitric acid to make the precipitate gel, and then reflux at 80°C 4h, a transparent sol can be prepared;
[0034] (iii) Preparation of Composite Sol
[0035] Mix the prepared silica sol with a mass concentration of 3% and the...
Embodiment 2
[0041] (1) Preparation of flame retardant composite sol-gel. The silica sol was synthesized from sodium silicate, the alumina sol was synthesized from aluminum isopropoxide, and then a silica-alumina composite sol was obtained by mixing the two.
[0042] (i) Silica sol preparation
[0043] Add 0.02mol sodium silicate and 60mL water into the reactor, stir vigorously at room temperature for 20min, then add 15ml of 37% hydrochloric acid dropwise, and continue vigorously stirring for 4h to obtain a stable, uniform and transparent silica sol;
[0044] (ii) Preparation of alumina sol
[0045] Add 0.03mol aluminum isopropoxide and 120mL water into the reactor, stir vigorously at 90°C, evaporate for 20-30min to remove most of the alcohol, slowly add 2ml of 95% nitric acid to make the precipitate gel, and then Reflux for 5 hours to obtain a transparent sol;
[0046] (iii) Preparation of Composite Sol
[0047] Mix the prepared silica sol with a mass concentration of 1.6% and the alu...
Embodiment 3
[0054] (1) Preparation of flame retardant composite sol-gel. The silica sol was synthesized from sodium silicate, the alumina sol was synthesized from aluminum isopropoxide, and then a silica-alumina composite sol was obtained by mixing the two.
[0055] (i) Silica sol preparation
[0056] Add 0.04mol sodium silicate and 100mL water into the reactor, stir vigorously at room temperature for 20min, then add 15ml of 36% hydrochloric acid dropwise, and continue vigorously stirring for 5h to obtain a stable, uniform and transparent silica sol;
[0057] (ii) Preparation of alumina sol
[0058] Add 0.03mol aluminum isopropoxide and 120mL water into the reactor, stir vigorously at 80°C, evaporate for 20-30min to remove most of the alcohol, slowly add 2ml of 95% nitric acid to make the precipitate gel, and then reflux at 80°C 4h, a transparent sol can be prepared;
[0059] (iii) Preparation of Composite Sol
[0060] Mix the prepared silica sol with a mass concentration of 2.1% and ...
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