Method and device for realizing carbon dioxide miscible-phase displacement laboratory experiment

A carbon dioxide and miscible flooding technology, applied in earthwork drilling, fluid extraction, sustainable manufacturing/processing, etc., can solve problems such as high minimum miscible pressure, restrictions on the development of carbon dioxide miscible flooding experiments, reduction of minimum miscible pressure by crude oil or carbon dioxide, etc.

Inactive Publication Date: 2015-11-11
NORTHEAST GASOLINEEUM UNIV
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Problems solved by technology

In order to evaluate the effect of miscible flooding and how to better realize miscible flooding in the mine, it is necessary to conduct laboratory experiments in advance. At present, the indoor experimental research of carbon dioxide flooding mainly includes carbon dioxide miscible flooding experiments and thin tube test minimum miscible pressure experiments, but the current laboratory memory Technical deficiencies in two aspects limit the development of corresponding carbon dioxide miscible flooding experiments
The corresponding technical defects are as follows: Technical defect 1, the short core used in laboratory experiments cannot realize the miscibility of carbon dioxide and crude oil in a short time, resulting in the inability to accurately evaluate the effect of complete miscible flooding
Technical defect 2, the pore throat size of the sand packing pipe in the thin tube test minimum miscible pressure experiment is not of the same order of magnitude as the actual core pore throat size, which makes the minimum miscible pressure tested by the device inaccurate
The reason is that the sand-packed tube is used to test the min

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  • Method and device for realizing carbon dioxide miscible-phase displacement laboratory experiment
  • Method and device for realizing carbon dioxide miscible-phase displacement laboratory experiment
  • Method and device for realizing carbon dioxide miscible-phase displacement laboratory experiment

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[0044] The present invention will be further described below in conjunction with the accompanying drawings:

[0045] Depend on figure 1 As shown, the device for realizing the carbon dioxide miscible flooding indoor experiment includes the following components, namely the thin tube drain valve 9, the core test control valve 10, the saturated oil thin tube valve 11, the liquid drain valve 12, the pressure holding valve 13, the thin tube Pipe valve 14, external equipment connector 15, constant pressure and constant speed pump for adding reagent 16, piston container 17, adding reagent storage tank 18, adding reagent flow totalizer 19, carbon dioxide flow totalizer 20, high temperature and high pressure visualization device 21, Conventional visualization slim tube 22, slim tube miscibility monitor 23, core miscibility monitor 26, saturated oil slim tube miscibility monitor 29, miscible phase monitor 30, natural core 24, core pressure monitor 25, slim tube pressure monitor 28, Pres...

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Abstract

The invention provides a method and a device for realizing a carbon dioxide miscible-phase displacement laboratory experiment, and mainly aims at solving the problem of technical bottleneck of the existing carbon dioxide miscible-phase displacement laboratory experiment. The method is characterized by comprising the following steps of: firstly preparing two visual fine pipes capable of completely simulating an actual rock core according to the actual rock core pore throat features; screening reagents through a high-temperature high-pressure visual device, determining a reagent capable of achieving a miscible-phase effect with carbon dioxide, and determining a miscible-phase pressure-volume curve of the carbon dioxide and an added reagent at different proportions; in the miscible-phase reaching range by a system, injecting the system into the visual fine pipes, and ensuring the carbon dioxide and the added reagent to perform the miscible-phase operation in pores; injecting the system achieving the miscible-phase goal into oil saturation visual fine pipes, regulating the injection proportion of the carbon dioxide and the added reagent in the miscible-phase range until the miscible phase of the system and crude oil is formed, and determining the injection proportion of the carbon dioxide and the added reagent and a pressure-volume curve of the system; and using the minimum miscible-phase pressure determined by a fine pipe experiment as the return pressure to inject the carbon dioxide and added reagent system at the proportion into the actual rock core so that the crude oil and the carbon dioxide realize the miscible phase.

Description

technical field [0001] The invention relates to a method and a device for an indoor experiment of miscible flooding in the technical field of improving oil well recovery by carbon dioxide flooding. Background technique [0002] Carbon dioxide flooding is currently a very promising method for enhancing oil recovery in tertiary oil recovery. Carbon dioxide flooding is divided into miscible flooding and immiscible flooding, and the oil displacement effect of miscible flooding is better than that of immiscible flooding. In order to evaluate the effect of miscible flooding and how to better realize miscible flooding in the mine, it is necessary to conduct laboratory experiments in advance. At present, the indoor experimental research of carbon dioxide flooding mainly includes carbon dioxide miscible flooding experiments and thin tube test minimum miscible pressure experiments, but the current laboratory memory Technical deficiencies in two aspects limit the development of corres...

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Application Information

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IPC IPC(8): E21B43/24
CPCY02P90/70
Inventor 刘丽皮彦夫刘英杰张继成张继红周志军万雪
Owner NORTHEAST GASOLINEEUM UNIV
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