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A high-performance sintered NdFeB rare earth permanent magnet material and its preparation method

A rare earth permanent magnet, NdFeB technology, applied in the direction of magnetic materials, inorganic material magnetism, magnetic objects, etc., can solve the problem of failing to meet the design requirements of the main phase, achieve small impact on remanence, improve coercivity, reduce The effect of boundary defects

Active Publication Date: 2017-06-13
NINGBO HUAHUI MAGNETIC IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the rare earth is reduced, it is easy to form α-iron, which cannot meet the main phase requirements of the design

Method used

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  • A high-performance sintered NdFeB rare earth permanent magnet material and its preparation method
  • A high-performance sintered NdFeB rare earth permanent magnet material and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] The first main phase magnetic powder alloy composition Nd 24 PR 6 co 1.8 Fe 61.1 Nb 0.6 al 0.30 Cu 0.2 B 1.0(mass percentage content), use the SC process to make flakes, use hydrogen explosion treatment to make the average particle size of the powder below 100 μm, and use hydrogen crushing and jet milling to make magnetic powder with an average particle size of 3.0-5.0 μm. Orientation press molding in 2T orientation magnetic field, isostatic pressing under 180MPa pressure. Sintering at 1050°C*2h, secondary heat treatment, 880°C*2h and 550°C*2h to obtain the first main phase sintered NdFeB magnet.

[0031] Alloy composition Dy of the second boundary zone structure 30 Fe 68.2 Nb 0.6 al 0.3 Cu 0.2 B 1.0 (mass percentage content), using the SC process to make flakes, using hydrogen explosion treatment to make the average particle size of the powder below 100 μm, and using hydrogen crushing and jet milling to make magnetic powder with an average particle size of...

Embodiment 2

[0037] The first main phase magnetic powder alloy composition Nd 24 PR 6 Fe 62.9 Nb 0.6 al 0.30 Cu 0.2 B 1.0 (mass percentage content), use the SC process to make flakes, use hydrogen explosion treatment to make the average particle size of the powder below 100 μm, and use hydrogen crushing and jet milling to make magnetic powder with an average particle size of 3.0-5.0 μm. Orientation press molding in 2T orientation magnetic field, isostatic pressing under 180MPa pressure. Sintering at 1050°C*2h, secondary heat treatment, 880°C*2h and 550°C*2h to obtain the first main phase sintered NdFeB magnet.

[0038] Alloy composition Dy of the second boundary zone structure 30 Fe 68.8 al 0.3 Cu 0.2 B 1.0 (mass percentage content), using the SC process to make flakes, using hydrogen explosion treatment to make the average particle size of the powder below 100 μm, and using hydrogen crushing and jet milling to make magnetic powder with an average particle size of 2.5-4.0 μm.

...

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Abstract

The invention relates to a high-performance sintered NdFeB rare earth permanent magnet material and a preparation method thereof. The material includes a first magnetic powder forming a main phase, a second magnetic powder forming a boundary region and a third magnetic powder forming a grain boundary phase. The preparation method includes: mixing according to the ratio that the second magnetic powder accounts for 0.1-10% of the total weight of the material, the third magnetic powder accounts for 1-15% of the total weight of the material, and the rest is the main phase alloy magnet prepared from the first magnetic powder, and is pressed. , Isostatic pressing, vacuum sintering and heat treatment, that is. The invention improves the boundary defects formed in the sintering process and makes the heavy rare earth elements as much as the boundary area as much as possible to improve the coercive force while minimizing the influence on the residual magnetism and improving the magnetic properties of the material; when obtaining equal magnetic properties Under the premise of significantly reducing the amount of heavy rare earth, reducing the cost.

Description

technical field [0001] The invention belongs to the field of sintered NdFeB rare earth permanent magnet materials, in particular to a high-performance sintered NdFeB rare earth permanent magnet material and a preparation method thereof. Background technique [0002] Sintered NdFeB permanent magnet materials are promoting computer hard disk technology, nuclear magnetic resonance imaging technology, electric vehicles, wind power generation, industrial permanent magnet motors, consumer electronics (CD, DVD, mobile phones, audio, copiers, scanners, video cameras, cameras, refrigerators) , TV sets, air conditioners, etc.) technology and the rapid development of magnetic machinery, magnetic levitation technology, magnetic transmission technology, etc. [0003] With the continuous expansion and deepening of the application market, the requirements for sintered NdFeB permanent magnet materials are also getting higher and higher. High performance and low cost. For this reason, new ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01F1/057H01F1/08B22F3/16
Inventor 钱勇
Owner NINGBO HUAHUI MAGNETIC IND
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