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Well cementation oil-based slurry flushing liquid and preparation method thereof

An oil-based mud and flushing fluid technology, applied in chemical instruments and methods, drilling compositions, etc., can solve problems such as difficulty in cleaning and affecting the quality of cementing at the two interfaces

Active Publication Date: 2016-02-10
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, these flushing fluids have certain limitations on the flushing effect of oil-based drilling fluid, especially when the plastic viscosity and shear force of the oil-based drilling fluid are high, the oil-based drilling fluid adhering to the casing wall and well wall It is difficult to clean it, which greatly affects the cementing quality of the second interface

Method used

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  • Well cementation oil-based slurry flushing liquid and preparation method thereof
  • Well cementation oil-based slurry flushing liquid and preparation method thereof
  • Well cementation oil-based slurry flushing liquid and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Add 0.2 parts of scleroglucan to 100 parts of water and stir for 50 minutes, then add 2 parts of polyoxyethylene alkylamine in turn (R1 is C16 alkyl; m, n=10), 3 parts of alkylphenol polyoxyethylene ether (R2 is an alkyl group of C9; x=10), 7 parts of alkyl alcohol polyoxyethylene ether carboxylate R 9 O(CH 2 CH 2 O) y CH 2 COOH (R9 is C16 alkyl; y=11), 4 parts of alkyl dihydroxyethyl carboxybetaine (R4 is C16 alkyl), 1.5 parts of Span 80, 1.5 parts of Tween 80.

example 2

[0038] Add 3.5 parts of Brunei gum to 100 parts of water and stir for 40 minutes, then add 3 parts of polyoxyethylene alkylamine in turn (R1 is C12 alkyl; m, n=8), 3 parts of alkylphenol polyoxyethylene ether (R2 is an alkyl group of C8; x=10), 5 parts of alkyl alcohol polyoxyethylene ether carboxylate R 9 O(CH 2 CH 2 O) y CH 2 COOH (R9 is C12 alkyl; y=7), 3 parts of alkyl dimethyl sulfonate betaine (R5 is C16 alkyl), 1 part of alkyl diisethionate betaine molecular formula is (R6 is C16 alkyl), 1.5 parts of Span 80, 1.5 parts of Tween 80.

example 3

[0040] Add 2.0 parts of Brunei gum to 100 parts of water and stir for 40 minutes, then add 3 parts of polyoxyethylene alkylamine in turn (R1 is C10 alkyl; m, n=6), 1 part of alkylphenol polyoxyethylene ether (R2 is an alkyl group of C12; x=12), 8 parts of alkyl alcohol polyoxyethylene ether carboxylate R 9 O(CH 2 CH 2 O) y CH 2 COOH (R9 is an alkyl group of C8; y=5), 5 parts of alkyl dimethyl carboxylate betaine molecular formula is (R3 is C12 alkyl), 2.0 parts of Span 80, 2.0 parts of Tween 80.

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Abstract

The invention discloses a well cementation oil-based slurry flushing liquid and a preparation method thereof. The flushing liquid comprises the components of, by weight, 100 parts of water, 4-8 parts of a nonionic surfactant, 5-8 parts of an anionic surfactant, 4-5 parts of an amphoteric surfactant, 1-2 parts of Span 80, 1-2 parts of Tween 80, and 0.2-3.5 parts of a tackifying and shear-strength-improving agent. The method comprises the following steps: according to the formula, the tackifying and shear-strength-improving agent is added, and the material is well mixed by stirring; the other components are added, and the mixture is well mixed by stirring, such that the well cementation oil-based mud flushing liquid is obtained. The flushing liquid provided by the invention has certain shearing strength and viscosity. Under the effect of hydraulic machinery, a dragging effect can be performed on oil slurry and oil films. Also, the flushing liquid has high emulsifying effects, and can be used for emulsifying the oil films and residual oil, such that viscose oil-based drilling fluid can be effectively cleaned. The flushing fluid is suitable to be used for flushing oil-based drilling fluid with high plastic viscosity and shearing force.

Description

technical field [0001] The invention relates to the field of oil field cementing, and more specifically, relates to an oil-based mud flushing fluid for well cementing and a preparation method thereof. Background technique [0002] Borehole wall instability brings certain difficulties to operations such as drilling, geological logging, logging and cementing. Oil-based drilling fluid is often used to solve shale stability problems, and has achieved good drilling results. However, as far as the cementing construction is concerned, the oil-based drilling fluid will stay at the interface and form oil slurry and oil film, which will seriously affect the interface bonding strength of the cement sheath and reduce the sealing quality of the cement sheath. Before operation, a flushing fluid with high-efficiency flushing effect should be injected to clean the oil slurry, oil film and mud cake adhering to the interface, improve the cementation environment of the annular space interface...

Claims

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Application Information

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IPC IPC(8): C09K8/524
Inventor 刘学鹏张明昌黄金营杨红歧张林海刘伟周仕明汪晓静
Owner CHINA PETROLEUM & CHEM CORP
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