Extraction method of infectious bronchitis egg yolk antibodies
A technology for bronchitis and chicken infectiousness, which is applied in the field of extraction of egg yolk antibody for chicken infectious bronchitis, can solve the problems of low yield and purity, and achieve the effects of strong biological activity, high purity and yield, and easy popularization and application
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0029] Take chicken eggs from hens immunized against infectious bronchitis, immerse them in 0.1% bromogeramine aqueous solution at 42°C for disinfection for 15 minutes, then immerse the eggs in water with a temperature above 95°C for 5 seconds, take them out and dry them in the air or blow them under aseptic conditions. Dry, beat the eggs to separate the egg white and yolk, fully remove the egg white and yolk mesangium, collect the yolk in a container, stir evenly, and obtain the egg yolk.
[0030] 1) Pretreatment of raw materials: Stir chicken yolk and purified water in a certain proportion evenly;
[0031] 2) Preliminary extraction of two-phase aqueous phase: slowly add 15% volume of saturated ammonium sulfate solution, add PEG to make the mass fraction reach 12%, stir for 20 minutes, let stand for 15 minutes, and collect the upper phase;
[0032] 3) Two-phase extraction and purification: slowly add 15% volume of saturated ammonium sulfate solution to the above solution, sti...
Embodiment 2
[0036] Take chicken eggs from hens immunized against infectious bronchitis, immerse them in 0.1% bromogeramine aqueous solution at 42°C for disinfection for 15 minutes, then immerse the eggs in water with a temperature above 95°C for 5 seconds, take them out and dry them in the air or blow them under aseptic conditions. Dry, beat the eggs to separate the egg white and yolk, fully remove the egg white and yolk mesangium, collect the yolk in a container, stir evenly, and obtain the egg yolk.
[0037] 1) Pretreatment of raw materials: Stir chicken yolk and purified water in a certain proportion evenly;
[0038] 2) Preliminary extraction of two-phase aqueous phase: slowly add 30% volume of saturated ammonium sulfate solution, add PEG to make the mass fraction reach 20%, stir for 30 minutes, let stand for 20 minutes, and collect the upper phase;
[0039] 3) Two-phase extraction and purification: slowly add 30% volume of saturated ammonium sulfate solution to the above solution, sti...
Embodiment 3
[0043] A method for extracting chicken infectious bronchitis egg yolk antibody, comprising the following steps:
[0044] 1) Take the egg yolk of chicken IBH-free, and mix it with water evenly in a ratio of 1:5 (v / v) to obtain the egg yolk dilution;
[0045] 2) Add 10% (v / v) saturated ammonium sulfate solution and PEG to the egg yolk dilution described in step 1) to obtain the first extraction system, then stir for 10 minutes, then let stand for 10 minutes, and collect the upper phase, which is the first upper extraction system Phase, the PEG content in the first extraction system is 8% (w / w);
[0046] 3) Add 10% (v / v) saturated ammonium sulfate solution to the first upper phase described in step 2) to obtain a second extraction system, then stir for 10 minutes, then let stand for 10 minutes, and collect the upper phase to be the second upper phase ; Add 10% (v / v) saturated ammonium sulfate solution to the second upper phase to obtain a third extraction system, adjust its pH t...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More