Additive for reinforcing reduction roasting of tin-containing materials to recover tin and method for separating and recovering tin from tin-containing materials
A technology of separation and recovery and additives, which is applied in the direction of improving process efficiency, etc., can solve the problems of high roasting temperature and long roasting time, and achieve the effects of efficient volatile recovery, low cost and reduced production cost
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[0028] Example 1:
[0029] Add additives to the tin-containing beneficiation tailings (TSn0.40%) with a particle size of -0.074mm accounting for 92% (the additives are composed of a mixture of 50% fluorite, 30% borax, and 20% sodium humate). Follow CaF 2 The molar ratio of Sn / Sn is 15:1. The additive is added to the finely ground material, mixed uniformly and then agglomerated and dried. The dried agglomerate is placed in a weak reducing atmosphere for reduction roasting, and the roasting temperature is 600°C. The roasting atmosphere is CO / (CO+CO 2 )=10%, roasting time 120min. The tin content in the roasting slag was analyzed to be 0.03%, and the tin volatilization rate was calculated to be 91.1%.
Example Embodiment
[0030] Example 2:
[0031] The tin iron ore (TSn0.71%) is crushed and ground to a particle size of -0.074mm, which accounts for 83%. Add additives to the finely ground materials (the additives are composed of 50% fluorite, 20% borax, 30% sodium humate mixed composition), the additive amount is in accordance with CaF 2 The molar ratio of Sn / Sn is 11:1. The additive is added to the finely ground material, mixed uniformly and then agglomerated and dried. The dried agglomerate is placed in a weak reducing atmosphere for reduction roasting at a roasting temperature of 725°C, The roasting atmosphere is CO / (CO+CO 2 )=30%, roasting time 15min. The tin content in the roasting slag is analyzed to be 0.08%, and the tin volatilization rate is calculated to be 90.2%.
Example Embodiment
[0032] Example 3:
[0033] The tin iron ore (TSn0.71%) is crushed and ground to a particle size of -0.074mm, which accounts for 83%. Add additives to the finely ground material (additives are based on the mass percentage of 60% fluorite, 20% borax, 20% % Sodium humate), the additive amount is in accordance with CaF 2 The molar ratio of Sn / Sn is 5:1. The additive is added to the finely ground material, mixed uniformly, agglomerated and dried, and the dried agglomerate is placed in a weak reducing atmosphere for reduction roasting at a roasting temperature of 750°C, The roasting atmosphere is CO / (CO+CO 2 )=19%, calcination time 55min. The tin content in the roasting slag was analyzed to be 0.07%, and the tin volatilization rate was calculated to be 91.7%.
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