Mg-Gd-Zn-Ni-Zr rare-earth magnesium alloy for semisolid forming and preparation method for semisolid blank of semisolid Mg-Gd-Zn-Ni-Zr rare-earth magnesium alloy
A technology for semi-solid forming and magnesium alloys, which is applied in the field of preparation of Mg-Gd-Zn-Zr magnesium alloys and semi-solid blanks, which can solve the problems of increased risk of oxidation and combustion of magnesium alloys, lower quality of finished magnesium alloys, and increased semi-solid Solve the problems of solid state forming energy consumption and production cost, and achieve the effects of high roundness of solid phase particles, low forming temperature, less oxidation and combustion
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Embodiment 1
[0024] Example 1: Mg-15Gd-2Zn-0.5Ni-0.3Zr alloy, wherein Gd: 15%, Zn: 2.0%, Ni: 0.5%, Zr: 0.3% (weight percentage), and the rest is Mg.
[0025] The preparation method of the semi-solid blank of the alloy comprises the following steps:
[0026] The first step, batching: use pure Mg, pure Gd, pure Zn, pure Ni and Mg-30wt.%Zr master alloy as raw materials, and batch according to the Mg-15Gd-2Zn-0.5Ni-0.3Zr alloy formula.
[0027] The second step, melting: After melting Mg, the temperature is raised to 750°C, after adding pure Gd, pure Zn, and pure Ni, then the temperature is raised to 780°C and kept for 120 minutes, and then the molten metal is evenly stirred; then the temperature drops to 750°C , add Mg-30wt.%Zr master alloy, keep warm for 30 minutes, and finally stir evenly to obtain a metal liquid with uniform composition.
[0028] The third step, solidification: heat the metal liquid obtained in the second step at 710°C for 10 minutes, then cool it at a cooling rate of 20...
Embodiment 2
[0031] Example 2: Mg-15Gd-2.8Zn-0.3Ni-0.5Zr alloy, wherein Gd: 15%, Zn: 2.8%, Ni: 0.3%, Zr: 0.5% (weight percentage), and the rest is Mg.
[0032] The preparation method of the semi-solid blank of the alloy comprises the following steps:
[0033] The first step, batching: use pure Mg, pure Gd, pure Zn, pure Ni and Mg-30wt.%Zr master alloy as raw materials, and batch according to the Mg-15Gd-2.8Zn-0.3Ni-0.5Zr alloy formula.
[0034] The second step, melting: After melting Mg, the temperature is raised to 750°C, after adding pure Gd, pure Zn, and pure Ni, then the temperature is raised to 780°C and kept for 120 minutes, and then the molten metal is evenly stirred; then the temperature drops to 750°C , add Mg-30wt.%Zr master alloy, keep warm for 30 minutes, and finally stir evenly to obtain a metal liquid with uniform composition.
[0035] The third step, solidification: heat the metal liquid obtained in the second step at 710°C for 10 minutes, then cool it at a cooling rate of ...
Embodiment 3
[0038] Example 3: Mg-15Gd-3.6Zn-0.7Zr alloy, wherein Gd: 15%, Zn: 3.6%, Zr: 0.7% (weight percentage), and the rest is Mg.
[0039] The preparation method of the semi-solid blank of the alloy comprises the following steps:
[0040] The first step, batching: use pure Mg, pure Gd, pure Zn and Mg-30wt.%Zr master alloy as raw materials, and batch according to the Mg-15Gd-3.6Zn-0.7Zr alloy formula.
[0041] The second step, melting: After melting Mg, the temperature is raised to 750°C, after adding pure Gd and pure Zn, then the temperature is raised to 780°C and kept for 120 minutes, and then the molten metal is evenly stirred; then when the temperature drops to 750°C, add Mg -30wt.% Zr master alloy, keep it warm for 30 minutes, and finally stir evenly to obtain a metal liquid with uniform composition.
[0042] The third step, solidification: heat the metal liquid obtained in the second step at 710°C for 10 minutes, then cool it at a cooling rate of 5°C / s, and obtain a master alloy...
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