Material for organic electroluminescent device and organic electroluminescent device
An electroluminescence device and electroluminescence technology, which are used in luminescent materials, electronic equipment, organic chemistry, etc. to achieve smooth charge transfer, improved life, and long life.
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[0085] Preparation
[0086] A method of synthesizing a material for an organic EL device and a method of manufacturing the organic EL device according to the present disclosure will be explained in more detail. However, the following examples are for illustration only, and the scope of the present disclosure is not limited thereto.
[0087] The synthetic method of compound 3
[0088] Compound 3 can be synthesized according to the following method. First, compound A was synthesized as an intermediate.
[0089]
[0090] Synthesis of Compound A
[0091] A solution of 8.00 g (30.9 mmol) of magnesium metal in 10 mL of dehydrated (eg, anhydrous) THF was added to a 500 mL three-necked flask, followed by stirring at about 0°C. A solution of 7.62 g (30.9 mmol) of 4-bromodibenzofuran in dehydrated THF was added dropwise, followed by stirring at room temperature for about 2 hours. A solution of 8.00 g (30.9 mmol) of 3-bromobenzophenone in 85 mL of dehydrated THF was added dropwis...
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