Material for organic electroluminescent device and organic electroluminescent device
An electroluminescence device and electroluminescence technology, which are used in luminescent materials, electronic equipment, organic chemistry, etc. to achieve smooth charge transfer, improved life, and long life.
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[0084] Example
[0085] Preparation
[0086] A method of synthesizing a material for an organic EL device and a method of manufacturing the organic EL device according to the present disclosure will be explained in more detail. However, the following embodiments are only for illustration, and the scope of the present disclosure is not limited thereto.
[0087] Synthesis method of compound 3
[0088] Compound 3 can be synthesized according to the following method. First, compound A is synthesized as an intermediate.
[0089]
[0090] Synthesis of compound A
[0091] A 10 mL dehydrated (for example, anhydrous) THF solution of 8.00 g (30.9 mmol) of magnesium metal is added to a 500 mL three-necked flask, followed by stirring at about 0°C. A dehydrated THF solution of 7.62 g (30.9 mmol) of 4-bromodibenzofuran was added dropwise, followed by stirring at room temperature for about 2 hours. A solution of 8.00 g (30.9 mmol) of 3-bromobenzophenone in 85 mL of dehydrated THF was added dropwise...
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