Pharmaceutical composition for treating gastric cancer and preparation method thereof
A kind of composition and medicine technology, applied in the field of pharmaceutical composition for treating gastric cancer and its preparation field
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Embodiment 1
[0025] Preparation of capsules
[0026] 1) Take vine root medicinal material and add ethanol with a mass fraction of 75% to heat and reflux for extraction twice. The amount of ethanol solution used each time is 12 times that of the raw material, and the extraction time is 3 hours, and the ethanol extract is combined. HPD-100 type macroporous adsorption resin was used for enrichment and purification, and the mass fraction of 45% ethanol was 12 times the amount of raw materials used for elution, and the elution rate was 6BV / h. The eluate was concentrated under reduced pressure to a thick paste with a relative density of 1.20-1.25 at 45°C, vacuum-dried at 35-45°C, -0.09mpa-0.10mpa, and pulverized to obtain the total flavonoids extract powder of total saponins of vine root, spare;
[0027] 2) Take Radix Astragali medicinal materials and add 60% ethanol to heat and reflux for extraction three times. The amount of ethanol solution used each time is 10 times the amount of raw materi...
Embodiment 2
[0031] Preparation of granules
[0032] 1) Take the vine pear root medicinal material and add 60% ethanol to heat and reflux for extraction 3 times. By weight, the amount of ethanol solution used each time is 10 times that of the raw material, the extraction time is 3 hours, and the ethanol extract is combined. HPD-100 type macroporous adsorption resin was used for enrichment and purification, and the mass fraction of 50% ethanol was 8 times the amount of raw materials used for elution, and the elution rate was 8BV / h. The eluate was concentrated under reduced pressure to a thick paste with a relative density of 1.20-1.25 at 50°C, vacuum-dried at 45-50°C, -0.09mpa-0.10mpa, and pulverized to obtain the total flavonoids extract powder of total saponins of vine root, spare;
[0033] 2) Take Radix Astragali medicinal materials and add 75% ethanol to heat and reflux for extraction twice. The amount of ethanol solution used each time is 10 times the amount of raw materials by weight...
Embodiment 3
[0037] Tablet preparation
[0038] 1) Take vine root medicinal material and add ethanol with a mass fraction of 50% to heat and reflux for extraction three times. The amount of ethanol solution used each time is 8 times that of the raw material, and the extraction time is 2 hours, and the ethanol extract is combined. HPD-100 type macroporous adsorption resin was used for enrichment and purification, and eluted with 60% ethanol with a mass fraction of 12 times the amount of raw materials, and the elution rate was 10BV / h. Concentrate the eluent under reduced pressure to a thick paste with a relative density of 1.20-1.25 at 50°C, vacuum-dry at 45-48°C, -0.08mpa-0.10mpa, and pulverize to obtain the total flavonoids extract powder of total saponins of vine root, spare;
[0039] 2) Take Radix Astragali medicinal materials and add 50% ethanol to heat and reflux for extraction three times. The amount of ethanol solution used each time is 12 times the amount of raw materials by weight...
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Abstract
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