Separator for nonaqueous secondary batteries, method for producing same and nonaqueous secondary battery
A secondary battery, non-aqueous technology, applied in the direction of non-aqueous electrolyte batteries, battery components, circuits, etc., can solve the problem of cycle life reduction and achieve high manufacturing efficiency
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[0164] Examples are given below to describe more concretely the separator and the non-aqueous secondary battery of the present disclosure. However, the separator and the non-aqueous secondary battery of the present disclosure are not limited to the following examples.
[0165]
[0166] The measuring methods used in each Example and Comparative Example are as follows.
[0167] [film thickness]
[0168] The film thickness (μm) of the porous substrate and the separator was determined by measuring 20 points using a contact-type thickness gauge (LITEMATIC manufactured by Mitutoyo Corporation), and calculating the average value. A cylindrical terminal with a diameter of 5 mm was used as a measurement terminal, and it was adjusted so that a load of 7 g was applied during the measurement.
[0169] The coating thickness (μm) of the porous layer was obtained by subtracting the film thickness of the porous substrate from the film thickness of the separator.
[0170] [Weight per unit...
Embodiment A1
[0191] A polyvinylidene fluoride-hexafluoropropylene copolymer (PVDF-HFP, KYNAR2800 manufactured by Arkema) was dissolved in a mixed solvent of acetone and water at a mass ratio of 95:5 to prepare a coating liquid. The concentration of PVDF-HFP in the coating liquid was 10% by mass.
[0192] Using a bar coater (bar coater) #6, the coating solution was applied to a polyethylene microporous membrane (thickness of 9.1 μm, Gurley value of 160 seconds / 100cc, porosity of 33 μm) as a porous substrate. %), forming coating layers on both sides of the porous substrate. This coating layer was dried at 60° C. to obtain a separator having porous layers on both surfaces of a polyethylene microporous membrane. The surface of the separator was observed with a scanning electron microscope (SEM), and it was confirmed that the porous layer had a honeycomb structure. The SEM image obtained by observing the surface of the separator from the vertical direction is shown in figure 1 .
Embodiment A2
[0194]Except having changed the mass ratio of acetone and water in a mixed solvent to 97.5:2.5, it carried out similarly to Example A1, and obtained the separator which has a porous layer on both surfaces of a polyethylene microporous membrane. The surface of this separator was observed by SEM, and it was confirmed that the porous layer had a honeycomb structure.
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