A kind of conductive paste for lithium ion battery and preparation method thereof
A lithium-ion battery, conductive paste technology, applied in battery electrodes, cable/conductor manufacturing, secondary batteries, etc., can solve the problems that are not particularly common, the use effect of conductive agents is not particularly ideal, and achieve the effect of improving conductivity
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Embodiment 1
[0022] Graphene functionalization
[0023] (1) Add 0.2g graphene oxide to 200mL NMP, and ultrasonicate for 2h;
[0024] (2) Add 0.6 g of octadecylamine, react in an oil bath at 120° C. for 48 hours, cool, dilute, filter with suction, put it in a vacuum oven and dry at 50° C. to obtain functionalized graphene.
[0025] Preparation of conductive paste
[0026] (1) Weigh 2g of sodium dodecylsulfonate and dissolve it in the solvent N-methylpyrrolidone, then add 6g of functionalized graphene to make a mixed solution, ultrasonicate for 5 hours, and filter with suction to obtain a solid;
[0027] (2) Weigh 1.5g PVDF, add 90g solvent N-methylpyrrolidone, stir evenly, and make a mixed solution;
[0028] (3) Weigh 3 g of carbon black, add the carbon black and the solid obtained by suction filtration into the above mixed solution, and stir for 10 hours with a high-speed shear disperser to obtain the conductive paste 1.
Embodiment 2
[0030] (1) Weigh 1.5g PVDF, add 90g solvent N-methylpyrrolidone, stir evenly, and make a mixed solution;
[0031] (2) Weigh 6 g of graphene and 3 g of carbon black, add the above mixed solution, and stir for 10 hours using a high-speed shear disperser to obtain conductive paste 2.
[0032] Table 1 is the performance test data of the conductive paste.
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