Cinnamon shower gel and preparation method thereof
A technology of shower gel and cinnamon, which is applied in the field of daily chemical industry, can solve the problems of consumers such as unclean cleaning, dryness, and high content of surfactant components, achieve good anti-inflammatory and anti-itching effects, remove dirt on the skin surface, and be hydrophilic and lipophilic good effect
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Embodiment 1
[0039] (1) Preparation of cinnamon essential oil: Take cinnamon bark, cinnamon leaves, and cinnamon seeds according to the ratio of mass ratio 1:1:1, mix and dry to constant weight, pulverize, pass through a 20-mesh sieve, and add the powdery material to the mixture with a mass of 2 1 times the mixed alcohol solution (concentration is that 90wt% methanol and 90wt% ethanol are mixed in a ratio of 1:2 by volume) as a carrier, through ultrasonically enhanced subcritical water extraction, separation, to obtain cinnamon essential oil; ultrasonically enhanced In the feed stage of subcritical water extraction, a pump is used to inject preheated deionized water into the extraction kettle at a flow rate of 70mL / min, and the liquid-material ratio is controlled to be 10:1mL / g; in the extraction stage, the ultrasonic frequency is 18.5Hz and the ultrasonic power is 100W , control the extraction pressure to 3MPa, the extraction temperature to 100°C, and the extraction time to 20min;
[0040...
Embodiment 2
[0043] (1) Preparation of cinnamon essential oil: take cinnamon bark, cinnamon leaves, and cinnamon seeds according to the ratio of mass ratio 1:2:2, mix and dry to constant weight, pulverize, pass through a 20-mesh sieve, and add the powdery material to the mixture with a mass of 3 1 times the mixed alcohol solution (concentration is that the methanol of 95wt% and the ethanol of 95wt% are mixed in the ratio of 1:3 by volume) as a carrier, and extracted by ultrasonically enhanced subcritical water, separated to obtain cinnamon essential oil; ultrasonically intensified In the feed stage of subcritical water extraction, a pump is used to inject preheated deionized water into the extraction kettle at a flow rate of 70mL / min, and the liquid-material ratio is controlled to be 20:1mL / g; in the extraction stage, the ultrasonic frequency is 18.5Hz and the ultrasonic power is 120W , control the extraction pressure to 5MPa, the extraction temperature to 110°C, and the extraction time to ...
Embodiment 3
[0047] (1) Preparation of cinnamon essential oil: take cinnamon bark, cinnamon leaves, and cinnamon seeds according to the ratio of mass ratio 1:3:4, mix and dry to constant weight, grind, pass through a 20-mesh sieve, and add the powdery material to the mixture with a mass of 4 1 times the mixed alcohol solution (concentration is that the methanol of 90wt% and the ethanol of 95wt% are mixed in the ratio of 1:4 by volume) as a carrier, and extracted by ultrasonically enhanced subcritical water, separated to obtain cinnamon essential oil; ultrasonically intensified In the feed stage of subcritical water extraction, a pump is used to inject preheated deionized water into the extraction kettle at a flow rate of 70mL / min, and the liquid-material ratio is controlled to be 30:1mL / g; in the extraction stage, the ultrasonic frequency is 18.5Hz and the ultrasonic power is 130W , control the extraction pressure to 7MPa, the extraction temperature to 130°C, and the extraction time to 50mi...
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