Preparation and application of polyiodide salt photoconductive material
A technology of photoconductive materials and iodized salts, which is applied in the field of photoconductive materials and polyiodized salt compounds, can solve the problems of high price and high toxicity of inorganic photoconductive materials, and achieve the effects of convenient post-processing, fast response time, and high photoconductive properties
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment example 1
[0030] The present invention provides the preparation method of the polyiodine 3-methylaminothiophene salt photoconductive compound, and its synthetic route is as follows Figure 9 as shown,
[0031] Specifically include the following steps:
[0032] Add hydrogen iodide aqueous solution and 3-methylaminothiophene to ethanol in a certain proportion, stir and place under light, let it stand for 12 to 24 hours, and then dry the solvent on a 40-degree hot table to obtain a dark brown solid. Wherein, the ethanol solvent can be other low-boiling polar solvents; the ratio between hydrogen iodide and 3-methylaminothiophene is 2:1.
Embodiment example 2
[0034] The preparation method of the polyiodomethylamino phenyl salt photoconductive compound is provided in the present invention, and its synthetic route is as follows Figure 10 as shown,
[0035] Specifically include the following steps:
[0036] Add hydrogen iodide aqueous solution and methylaminobenzene to ethanol in a certain proportion, stir and place under light, let it stand for 12 to 24 hours, and then place it on a 40-degree hot table to dry the solvent to obtain a dark brown solid. Wherein, the ethanol solvent can be other low-boiling polar solvents; the ratio between hydrogen iodide and methylaminobenzene is 2:1.
Embodiment example 3
[0038] The present invention provides the preparation method of the polyiodine 3-methylaminothiophene salt photoconductive compound, and its synthetic route is as follows Figure 11 as shown,
[0039] Specifically include the following steps:
[0040] Add sodium iodide, simple iodine and 3-methylaminothiophene to ethanol in a certain proportion and stir, adjust the pH of the solution to 1-4 with hydrochloric acid, dry the solvent at 50-60 to obtain a dark brown solid. Wherein, the ethanol solvent can be other low-boiling polar solvents; the iodine salt can be NaI, KI, HI. The ratio of iodine salt to simple iodine is 1:1, and the ratio between the total iodine content and 3-methylaminothiophene is 3:1 to 2:1.
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 


