3627results about How to "Easy post-processing" patented technology

Methods for generating supports (30) for parts (50) produced by solid freeform fabrication (“SFF”) are disclosed. The method includes defining a plurality of layers (L) that make up the part, and for each layer, determining those regions (R) that require support. The method also includes merging the regions for the different layers (L) into one or more common regions that require support, and providing at least one support for each of the one or more common regions. The result is that fewer supports are used as compared to conventional SFF fabrication methods.

A device for separating water from sludge comprising a processing box, wherein a feeding cylinder is disposed above the processing box, and the feeding cylinder is fixedly connected to the processing box through a plurality of connecting rods; a rotating rod is rotationally connected into the feeding cylinder; a first rotating motor is fixedly connected to one side of the feeding cylinder; the output end of the first rotating motor penetrates through the side wall of the feeding cylinder, and is fixedly connected to the rotating rod; a spiral blade is fixedly sleeved with the rotating rod, and the outer side of the spiral blade is matched with the inner side wall of the feeding cylinder.

The invention discloses a method for 3D reconstruction and texture generation from single-view face based on multi-task learning, belonging to the computer vision field. The method comprises the following steps of: selecting a special viewpoint for rendering a three-dimensional human face model; generating depth map and texture map as truth value data from special viewpoint; designing an integrated learning and coding network based on feature sharing of depth information and texture information; designing the branch decoding network to recover the depth map from the shared features, and recovering the depth map, designing the mutual information with shared features as latent variables to maximize the generation of antagonistic network, and restoring the texture unwrapping map, adjusting the proportion of each task loss function and training the model; interpolating the depth map and using texture map to reconstruct the 3D face mesh model with texture details. The invention utilizes multi-task learning to carry out single-view face three-dimensional reconstruction, texture generation and style migration, and has the advantages of high speed, low cost and the like.

The invention relates to a reactive dye ultra-short rapid dyeing and fixation technology method. The method is realized by effectively minimizing auxiliary time such as feeding, shortening and optimizing post-processing processes, especially carrying soap boiling (one bath color mending) only once in advance to the greatest extend, merging washing, using less hot water and controlling the use of water aiming at various substances to be dyed according to dyeing requirements and the conditions of normal or abnormal and with the help of various accessory ingredients, thereby the reactive dye normal or abnormal dyeing conditions (especially mediate high color with a dye usage higher than 1percent of o. W. f) by the single one bath process, the multifunction composite one bath process, or the like, comprising pre-processing, dyeing, polishing with enzyme, and color mending, and even the pre-processing and the whole dyeing procedure in conventional equipment in an ultra-low bath ratio limit state can be completed well within 2.5-8h. The effects of thorough energy saving and emission reduction, efficiency increasing and consumption reduction, cleaner production and environmental protection are achieved.

The invention discloses a preparation method for a phenanthridine derivative. The preparation method comprises the following steps of: adding a catalyst, an oxidant, acid, a 2-phenylaniline compound and an olefin compound into organic solvent; after reaction, carrying out post treatment to obtain the phenanthridine derivative, wherein the catalyst is a bivalent palladium catalyst. According to the preparation method for the phenanthridine derivative disclosed by the invention, the adoption of reagents with high toxicity and high corrosiveness is avoided. The preparation method has the advantages of environment friendliness, easiness in operation, higher yield and simplicity and convenience in post treatment. In addition, a substrate obtained by the method is strong in designability and can be used for designing to synthesize a compound with the required structure according to actual requirements, and thus stronger practicability is realized.

A combined interference device for measurement of aspheric surface includes a laser, a spatial filter, two beam expanding systems, a beam shrinking system, a spectroscope, a convertible lens, three polarizers, two optical plates, four circular optical wedges with small wedge angle, a beam-dividing grating, a 1/4 wave plate, a polarizer group and a CCD. In the device, real-time measurement is realized through simultaneous phase-shifting method, and frequency conversion function is realized through rotating two pairs of double optical wedges. The experimental device adopts common optical elements, so the cost is low, and the device can measure aspheric surfaces of different diameters and is suitable for the plane and the sphere. The real-time high precision measurement in conventional environment can be realized, and the invention has frequency conversion function, which is very effective for treating the mirror surface with discontinuous regions.

An inspection method for detecting a defect in a test object. A particulate is generated, then the generated particulate is introduced into a test object. Subsequently, light having high directivity is emitted such that the light passes in the vicinity of the test object to irradiate the particulate discharged from the test object, thereby making the particulate visible. An inspection apparatus for detecting a defect in a test object, including a particulate generating means for generating a particulate, a particulate introducing means for introducing the particulate into a test object, and a light emitting means for emitting light with high directivity that passes in the vicinity of the test object and irradiates the particulate discharged from the test object thereby to visualize the particulate. The inspection method and apparatus detect a defect of a test object with high sensitivity, permit easier identification and recording of the location of a defect, and shorten an inspection time and the time required for the pre-treatment and post-treatment before and after an inspection, or obviate the need for the pre-treatment and post-treatment.

An extrusion process comprises extruding a material that is flowable when heated and passing the extrudate thus formed through a nozzle 10 to shape the extrudate into a plurality of substantially uniformly shaped elements such as minispheres or minicapsules.

The invention relates to a method for preparing a high-nickel long-cycle single-crystal nickel-cobalt-manganese (NCM) lithium ion battery positive-pole material. The preparation method comprises the following steps: (1) mixing a soluble nickel salt, a cobalt salt, a manganese salt, an alkali metal hydroxide and ammonia water, and enabling the mixture to flow into a reaction kettle for constant-temperature coprecipitation to obtain a high-nickel NCM ternary precursor material; (2) uniformly mixing the high-nickel NCM ternary precursor, lithium hydroxide and an additive A in a wet high-speed mixing mode, carrying out drying, then carrying out primary sintering in an oxygen-enriched atmosphere to obtain a spherical high-nickel NCM ternary positive-pole material; (3) carrying out crushing, smashing and sieving to obtain a high-nickel NCM ternary positive-pole material; and (4) carrying out wet mixing and drying on the high-nickel NCM ternary positive-pole material with a coating agent B, carrying out secondary sintering in an oxygen-enriched atmosphere, and carrying out crushing, smashing and sieving to obtain the high-nickel single-crystal NCM lithium ion battery positive-pole material. The positive-pole material prepared by the method has the advantages of high capacity, good cycle performance, high compaction density and the like.

The invention discloses a reactive phosphorus flame retardant containing DOPO and an active double bond and a preparation method and application thereof. Dichloro replaces phosphate to react with polyhydric alcohols or polyhydric phenol acidifying with propylene or partial methyl propene and then with DOPO modified aryl-dihydric phenol and DOPO modified aryl-dihydric alcohol, and a reactive flame retardant monomer molecule capable of being cured and provided with active double bonds and a DOPO flame retardant group are obtained and can be used in various flame retardants of epoxyacrylates and unsaturated polyester resins and the like containing unsaturated double bond polymer resins. The flame retardant overcomes defects that the compatibility between an additive flame retardant and a matrix is poor, the additive flame retardant and the matrix are easy to lose, the water resistance is poor, and the like, and the LOI (limit oxygen index) value of resins can be improved remarkably and the flame-resistant effect is good when the flame retardant is used for flame retarding in the epoxyacrylates and the unsaturated polyester resins.

The invention relates to a balancing lead smelting process for comprehensive resource utilization and a device thereof. The process comprises the following steps: granulating a raw material containing lead and a fluxing agent after proportioning, sending to an oxygen bottom-blown smelting furnace for smelting to produce primary crude lead, lead ash and flue gas of SO2; sending the flue gas of SO2 to a sulfuric acid system for acid making after recovering waste heat by a waste heat boiler and duct collection by a dust arrester installation; adjusting form of the lead ash and adding the lead ash to a blast furnace together with coking coal for reducing smelting to produce secondary and third crude lead; electrorefining the crude lead to obtain refined lead and anode slime, treating and recovering the anode slime to obtain lead, stibium, bismuth, gold and silver metals; and separating slag of the blast furnace from the crude lead and sending to a fuming furnace to recover zinc oxide, the lead, indium and germanium. A system for realizing the process comprises the oxygen bottom-blown smelting furnace, an oxygen lance, an electrically-heated settler, a slag casting device, the waste heat boiler with a vertical ascending segment of membrane wall structure, the blast furnace, the fuming furnace and a ventilating device. The process design and system improvement help realize balancing optimized recovery of Pb, Zn, Au, Ag, Bi, Cu, In, Sb and S elements.

The invention discloses a cardanol-based antioxidant as well as a preparation method and application thereof. The cardanol-based antioxidant contains a compound with a structure shown as a formula (1): (shown in the description), wherein n ranges from 0 to 3; R1 and R2 are respectively and independently selected from H, alkyl, cycloalkyl, aryl, alkaryl or aralkyl; at least one of R3 and R4 has a structure shown as a formula (2) or (3): (shown in the description); R and R' are respectively and independently selected from H, alkyl, cycloalkyl, aryl, alkaryl or aralkyl; R5 is selected from -S-, -O-, -NH- or -(CH2)n'-; n' ranges from 0 to 3; Ra and Rb are respectively and independently selected from H, -OH, -SH, -NH2, alkyl, cycloalkyl, aryl, alkaryl or aralkyl; m and m' are any integer of 0 to 3 respectively. The cardanol-based antioxidant disclosed by the invention has the characteristics of greenness, environmental protection, antioxidation property, excellent thermal stability and extreme pressure resistance and the like; a preparation process has the advantages of simplicity, feasibility, mild conditions and wide application prospect in the fields of multiple oil products, fuel, plastic, rubber, fibers, coatings and the like.

The invention discloses facility for automatically collecting waste liquid in volumetric flasks. The technical scheme of the facility includes that the facility for automatically collecting waste liquid comprises a fixing device, a power transmission device, a single-shaft robot, a transportation device and a rotary fixture. A container containing waste liquid is arranged on the fixing device, the fixing device on a conveyor is driven by a motor to be conveyed to an operation table, a cover of the container is unscrewed and placed in a cover collecting disc by a manipulator, the fixing device is transported to the rotary fixture above a waste liquid collecting barrel by a sucker, is fixed in a fixed sleeve, is turned and shaken by a rotating cylinder so that the waste liquid can be poured out, and finally is transported to the conveyor to be moved out of the operation table. The facility for automatically collecting waste liquid is simple in structure, convenient to operate, labor-saving, material-resource-saving, time-saving, safe, quick, high-efficient and automatic. Frequent working procedures are avoided.

The invention discloses preparation of hydrophilic polymer and application thereof in detecting mercury ions based on the change of fluorescence and color, particularly a rhodamine B hydrazide grafted hydrophilic polymer probe applied to the detection of mercury ions in aqueous medium based on the change of fluorescence and color and a kit and test paper applied to the detection of the mercury ions by using the probe, belonging to the technical field of material preparation and heavy metal ion detection. The polymer containing a rhodamine chromophore is prepared by subjecting rhodamine B hydrazide and propylene oxide on the side chain of polyvinylpyrrolidone-glycidyl methacrylate which is a water-soluble polymer to ring-opening reaction, has good water solubility and can be applied to selectively detecting the mercury ions by using visual colorimetry and fluorescence detection. The probe realizes the high-sensitivity and high-selectivity rapid quantitative or semi-quantitative detection of the trace mercury ions in the aqueous medium, has a simple synthetic route, low cost and convenience of use, is applicable to amplified synthesis and actual production and has great application prospects in the field of medicine, biology and environmental science and the like.

The invention relates to a preparation method of 2, 5-disubstituted thiophene compound I and the usage of the 2, 5-disubstituted thiophene compound in preparation of compound V. The preparation method is used for synthesizing the compound I by a 'one-pot' method through compound II and compound III under the condition that sulfur reagent exists. Compared with the prior art, the invention has the advantages of being easy in material obtaining, mild in reaction condition, simple and convenient in operation, high in yield, suitable for industrialized production and the like.

The invention relates to a synthesis technique of tenofovir, and relates to the field of medicinal chemistry. Using natural (R)-lactate as the starting material, chiral R-1,2-propanediol is obtained through reduction, and then reacted with diethyl carbonate under the action of alkali to obtain the key reaction intermediate R-propylene carbonate ester. Use adenine and R-propylene carbonate to prepare R-9-(2-hydroxypropyl)adenine; Gained R-9-(2-hydroxypropyl)adenine and diethyl p-toluenesulfonyloxyphosphate Under the catalysis of magnesium tert-butoxide, the condensation reaction is carried out to obtain R-9[(diethylphosphorylmethoxy)propyl]purine; the obtained R-9[2-(diethylphosphorylmethoxy) Propyl]purine is hydrolyzed to obtain Tenofovir. The process has short reaction steps, short required reaction time, high quality yield and good product quality, and is suitable for industrialized production.

The invention discloses an esterifiable modification method of lignocelluloses and esterifiable modified lignocelluloses. The esterifiable modification method comprises the following steps: dissolving lignocelluloses in an ionic liquid; and carrying out esterification reaction on the lignocelluloses and an esterifying agent. The method disclosed by the invention has the characteristics that the prices of the used raw materials are low, the technologic process is simple, the reaction process has no pollution, a reaction system can be reused, the hydroxyl substitution degree of a prepared lignocellulose esterification material can be controlled, and the like; and the method is one of important methods for industrial transformation and utilization of renewable lignocellulose resources.

The invention relates to a conveying device, in particular to a logistics conveying device. The logistics conveying device can save time and labor and is low in labor intensity, capable of detecting express packages and high in working efficiency. The logistics conveying device comprises a base plate and the like. A conveying device body is arranged at the top of the base plate. A collection box is arranged on the left side of the base plate and located below the left side of the conveying device body, and buffering devices are arranged in the collection box. According to the logistics conveying device, through a first detection device and a first conveying belt, the express packages can be conveyed and can also be detected in the conveying process, and the effects of time saving, labor saving and low labor intensity are achieved; and the express packages can be detected, so that the effects of time saving, labor saving and low labor intensity are further achieved; and the conveying device can detect the express packages and thus also has the effect of high working efficiency.

The invention relates to a preparation method of inert alkyl reversed phase silica gel chromatographic filler, which belongs to the technical field of high performance liquid phase chromatography. The invention comprises the following steps: step 1 of getting silica gel particles with hydroxyl on the surface through acidification pretreatment of silica gel matrix particles; step 2 of hydroxylation of the silica gel matrix particles, and getting the alkyl reversed phase silica gel filler by making use of corresponding alkyl silicane reagents and by adopting a method of liquid phase reaction to make surface alkyl treatment to the acidification pretreated silica gel particles with the hydroxy; step 3 of inert treatment of the alkyl silica gel matrix filler, and putting the prepared dry alkyl reversed phase silica gel filler into an autoclave with a certain volume, adding a certain amount of silicane terminated reagents and sealing the autoclave to make seal terminated reaction in the inert gas atmosphere to obtain the highly inert alkyl reversed phase silica gel chromatographic filler. In appropriate chromatographic conditions, the filler prepared in the invention can be effectively used in the separation analysis of acidic, neutral and basic compounds.

The invention relates to a preparation method of a magnetic cadmium ion surface imprinted polymer, which comprises the following steps: synthesizing magnetic Fe3O4@SiO2 microspheres through a coprecipitation method and a sol-gel method, and treating with acid to increase the surface hydroxyl content; introducing polymerizable double bonds onto the surfaces of the Fe3O4@SiO2 microspheres through a two-step method, namely grafting amino groups onto the surfaces of the microspheres by using aminosilane coupling agent, and generating the double bonds through reaction between acid anhydride and the amino groups; and finally, performing polymerization reaction by taking the Fe3O4@SiO2 microspheres as carriers, taking Cd(II) as a template, taking ethylene glycol dimethacrylate as crosslinking agent and taking methacrylic acid and salicylaldoxime as monomers, and washing off the template Cd(II) after the reaction, thus obtaining a polymer layer with a large number of Cd(II) imprinted holes distributed on the surfaces of the Fe3O4@SiO2 microspheres. The magnetic cadmium ion surface imprinted polymer provided by the invention can be used for separation and removal of cadmium ions.

The invention discloses a bicolor Eu-MOFs/CDs fluorescent material as well as preparation and an application thereof. Europium ions, trimesic acid and carbon quantum dots are used as raw materials, and the bicolor fluorescent material is prepared through heat treatment in a solvent prepared by mixing N,N-dimethylformamide, distilled water and cyclohexanol. Under irradiation of ultraviolet lamps, the material can emit red fluorescence when dispersed in organic solvents and can emit blue fluorescent when dispersed in water, so that fluorescent colorimetric sensors for measuring water content in organic solvents can be prepared from the material, the prepared sensors are high in sensitivity, good in stability and low in cost and have higher population value and brighter application prospect.

The invention discloses a Fe2O3 micro-nano porous sphere, a preparation method thereof and uses thereof. The porous sphere is formed by Fe2O3 nanoparticles having a nanometer mesoporous alpha-Fe2O3 phase structure therebetween, wherein the diameter of the sphere is 500-5000nm, the specific surface area of the sphere is 15-25m<2>/g, particle sizes of the particles are 20-60nm, and pore diameters of mesopores are 2-50nm. The method comprises the following steps: mixing ferric chloride hexahydrate, ascorbic acid, urea and water, and uniformly stirring them to obtain a mixed liquid; reacting the mixed liquid under conditions that the temperature is 140-180DEG C and the pressure is a self-generated pressure for at least 4h to obtain an intermediate product; separating, washing and drying the intermediate product to obtain porous iron carbonate; and annealing the porous iron carbonate at 450-550DEG C for at least 4h, and naturally cooling the porous iron carbonate to room temperature to prepare the Fe2O3 micro-nano porous sphere. The Fe2O3 micro-nano porous sphere can be placed in water polluted by organic dyes to photocatalytically degrade under visible light, or in water polluted by potassium dichromate to adsorb.

The invention provides a method for detecting any defect in the inner wall of a hole by an optic way, which comprises the following procedures: a light pickup picks up an image formed by laser after reflecting on the inner wall of the hole, so as to get the depth at any point on the inner wall of the hole; the light pickup picks up an image formed by an illumination light after reflecting on the inner wall of the hole, so as to get the explored image of the inner wall of the hole and get the 2D sizes of the defect; and the 3D info on the defect is obtained by combining above two dimensions. By combining laser measurement with illumination light measurement, it is not only possible to get the 2D size of the defect, but also is possible to get the depth of the defect, so as to achieve 3D measurement of the defect; the use of a non-contact measuring way avoids any contact wear between a probe and the object to be measured, and improves the inspection speed.