The invention discloses a near-neutral synthesis method of high-aluminum-content mesoporous
aluminosilicate, which comprises the following steps: firstly, dissolving a template agent in deionized water, and fully stirring to obtain a uniform template agent solution; the preparation method comprises the following steps: uniformly mixing a
silicon source with an inorganic salt, and uniformly mixing an aluminum source with a dilute
sulfuric acid solution in deionized water to prepare a
silicate solution and an aluminum
salt solution; synchronously dripping the
silicate solution and the aluminum
salt solution into the template agent solution to form an
aluminosilicate precursor; and performing
crystallization, suction
filtration, washing,
drying and
roasting treatment on the precursor to finally obtain the mesoporous
aluminosilicate material. In the process of synthesizing the mesoporous aluminosilicate by using the inorganic salt under the near-neutral condition, anions and aluminum ions form a soluble complex (such as Al (HCO3) 2 +), hydrolytic
precipitation of aluminum species in a neutral environment is effectively inhibited, and it is ensured that the
aluminum element participates in the reaction in an active form; the efficient synthesis of the mesoporous aluminosilicate material with
high aluminum content and high order degree is realized.