Method for preparing flexible iron sesquioxide/ferroferric oxide and nitrogen doped carbon composite nano-fibers
A technology of composite nanofiber and ferric oxide, applied in fiber treatment, fiber chemical characteristics, rayon manufacturing, etc., can solve the problems of complex and harsh conditions, high cost, difficult mass production, etc., achieve low cost, inhibit agglomeration, evenly distributed effect
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[0034] Embodiment: A kind of preparation method of flexible ferric oxide / iron tetroxide and nitrogen-doped carbon composite nanofiber is specifically completed according to the following steps:
[0035]1) Preparation of metal-organic gel and polyacrylonitrile mixed solution: add polyacrylonitrile to DMF to dissolve, and configure a solution with a mass concentration of polyacrylonitrile of 0.1g / mL; at room temperature, at a stirring speed of 300r / min , add ferric nitrate nonahydrate solid to the above solution, so that the mass ratio of ferric nitrate nonahydrate and polyacrylonitrile is 1:1, stir and mix thoroughly for 2 hours; then add a certain amount of 1,3,5-benzenetricarboxylic acid in DMF solution, wherein the molar ratio of 1,3,5-benzenetricarboxylic acid to ferric nitrate nonahydrate was 1:1.5, and continued to stir for 3 minutes to obtain a mixed solution of metal-organic gel and polymer. 2) Preparation of flexible metal-organic gel and polyacrylonitrile composite na...
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