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Preparation method of quasi-solid electrochromic device

An electrochromic device and electrochromic technology, applied in the direction of instruments, nonlinear optics, optics, etc., can solve the problems of few reports on the preparation process of quasi-solid-state electrochromic devices, so as to avoid the influence of device performance and stabilize the process , The effect of high controllability of finished product quality

Active Publication Date: 2017-07-18
JIANGSU FANHUA GLASS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] After searching, there are many reports on the preparation process of all-solid-state electrochromic devices, but there are few reports on the preparation process of quasi-solid-state electrochromic devices

Method used

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  • Preparation method of quasi-solid electrochromic device
  • Preparation method of quasi-solid electrochromic device
  • Preparation method of quasi-solid electrochromic device

Examples

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preparation example Construction

[0034] The preparation method of the quasi-solid-state electrochromic device of the present invention, such as figure 1 As shown, the device is sequentially composed of a first substrate 1, a first transparent conductive layer 2, an electrochromic layer 3, an ion transport layer 4, an ion storage layer 5, a second transparent conductive layer 6 and a second substrate 7; The preparation method comprises the following steps:

[0035] (1) Prepare the first functional substrate, such as figure 2 as shown,

[0036] Step 1: Use a clean and highly transparent material as the first substrate 1, and form a conductive silver paste with a thickness of 300-400 um on the surface of the first substrate 1 through a silk screen printing process, as an electrode, and then uniformly spread the conductive silver paste on the surface of the conductive silver paste Deposit a layer of transparent conductive film with a film thickness of 20-400nm to form the first transparent conductive layer 2; ...

Embodiment 1

[0056] The preparation method of the PMMA / PVB gel quasi-solid-state electrochromic device containing lithium ions in this embodiment comprises the following steps:

[0057] (1) Preparation of the first functional substrate:

[0058] Step 1: Use clean plexiglass as the first substrate 1, and form a conductive silver paste with a thickness of 300-400 um on the surface of the first substrate 1 through a silk screen printing process as an electrode. The screen printing process uses a 200-mesh screen printing screen cloth, the distance between the screen printing mesh and the first substrate is 2-4mm, and the screen printing pressure is 1.5-3bar; then a layer of transparent conductive film with a film thickness of 20-400nm is evenly deposited on the surface of the conductive silver paste by vacuum coating process, and the deposition The temperature is 350-380°C, the deposition power is 12-14kw.h, the transmission speed is 0.8-1.2m / min, and the reaction pressure is 0.5-0.6pa to form...

Embodiment 2

[0071] The preparation method of the PMMA / PVB gel quasi-solid-state electrochromic device containing lithium aluminum ions in this embodiment comprises the following steps:

[0072] (1) Preparation of the first functional substrate:

[0073] Step 1: Use clean plexiglass as the first substrate 1, and form a conductive silver paste with a thickness of 300-400 um on the surface of the first substrate 1 through a silk screen printing process as an electrode. The screen printing process uses a 200-mesh screen printing screen cloth, the distance between the screen printing mesh and the first substrate is 2-4mm, and the screen printing pressure is 1.5-3bar; then a layer of transparent conductive film with a film thickness of 20-400nm is evenly deposited on the surface of the conductive silver paste by vacuum coating process, and the deposition The temperature is 350-380°C, the deposition power is 12-14kw.h, the transmission speed is 0.8-1.2m / min, and the reaction pressure is 0.5-0.6p...

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Abstract

The invention relates to a preparation method of a quasi-solid electrochromic device. The device consists of a first substrate, a first transparent conductive layer, an electrochromic layer, an ion transmission layer, an ion storage layer, a second transparent conductive layer and a second substrate sequentially. The preparation method comprises the following steps: (1) preparing the first functional substrate; (2) preparing the second functional substrate; (3) preparing the ion storage layer; (4) performing alignment heating and laminating; (5) removing bubbles by a high-pressure kettle; and (6) gluing frames. The preparation method of the quasi-solid electrochromic device has the advantages of simple method, low investment cost, high quality controllability of finished products, and high color-changing uniformity, and can realize large-area industrialized production.

Description

technical field [0001] The invention belongs to the field of electrochromic devices, in particular to a quasi-solid-state electrochromic [0002] Device fabrication method. Background technique [0003] Electrochromism refers to the phenomenon that optical properties (reflectivity, transmittance, absorptivity, etc.) undergo a stable and reversible color change under the action of an applied electric field. Electrochromic technology has been developed for more than 40 years. Electrochromic devices (Electrochromic Device, ECD) are widely used in smart windows, It has broad application prospects in fields such as displays, spacecraft temperature control and modulation, automotive non-glare rearview mirrors, and weapons and equipment stealth. [0004] Electrochromic devices generally have a five-layer structure: a transparent conductive electrode layer, an electrochromic material layer, an electrolyte layer, an ion storage layer, and another conductive electrode layer. At pre...

Claims

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Application Information

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IPC IPC(8): G02F1/15G02F1/153G02F1/161
CPCG02F1/15G02F1/1523G02F1/153G02F1/161
Inventor 刘江王群华刁训刚张帆吉顺青叶书兵童伟
Owner JIANGSU FANHUA GLASS CO LTD
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